trans-[RuCl₂(2-(N,N-dimethylamino)methylpyridine)(1,1'-bis(diphenylphosphino)ferrocene)]

Base Information

• Chemical Name: trans-[RuCl₂(2-(N,N-dimethylamino)methylpyridine)(1,1'-bis(diphenylphosphino)ferrocene)]
• CAS No.: 1315461-20-1
• Molecular Formula: C₄₂H₄₀Cl₂FeN₂P₂Ru
• Molecular Weight: 862.564

Synonyms:

Chemical Property of trans-[RuCl₂(2-(N,N-dimethylamino)methylpyridine)(1,1'-bis(diphenylphosphino)ferrocene)]

Chemical Property:

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Technology Process of trans-[RuCl₂(2-(N,N-dimethylamino)methylpyridine)(1,1'-bis(diphenylphosphino)ferrocene)]

There total 1 articles about trans-[RuCl₂(2-(N,N-dimethylamino)methylpyridine)(1,1'-bis(diphenylphosphino)ferrocene)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

1,1'-bis-(diphenylphosphino)ferrocene (12150-46-8) + 2-[(Dimethylamino)methyl]pyridine (43071-19-8) + dichlorotetrakis(triphenylphosphine)ruthenium(II) (15555-77-8,86470-43-1) → trans-[RuCl2(2-(N,N-dimethylamino)methylpyridine)(1,1'-bis(diphenylphosphino)ferrocene)] (1315461-20-1)

Guidance literature:

In toluene; mixt. of Ru complex and NC5H4CH2NMe2 in toluene was heated to 110°C for 1 h in Schlenk flask under N2; cooled; Fe complex was added; heated to 110°C for 19 h; cooled to room temp.; pentane added; cooled in ice bath; filtered; supernatant concd. (vac.); treated with pentane; filtered; elem. anal.;

DOI:10.1021/om2004755

upstream raw materials:

1,1'-bis-(diphenylphosphino)ferrocene

2-[(Dimethylamino)methyl]pyridine

dichlorotetrakis(triphenylphosphine)ruthenium(II)

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