((S)-1-Allyloxy-2,2,2-trichloro-ethyl)-carbamic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester

Base Information

• Chemical Name: ((S)-1-Allyloxy-2,2,2-trichloro-ethyl)-carbamic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester
• CAS No.: 126442-14-6
• Molecular Formula: C₂₈H₄₅Cl₃N₂O₅S
• Molecular Weight: 628.101

Synonyms:

Chemical Property of ((S)-1-Allyloxy-2,2,2-trichloro-ethyl)-carbamic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of ((S)-1-Allyloxy-2,2,2-trichloro-ethyl)-carbamic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester

There total 10 articles about ((S)-1-Allyloxy-2,2,2-trichloro-ethyl)-carbamic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Carbamic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester (121666-42-0) → ((R)-1-Allyloxy-2,2,2-trichloro-ethyl)-carbamic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester (126442-14-6,126575-75-5)

Guidance literature:

Multi-step reaction with 3 steps

1: benzene / 20 h / Heating

2: thionyl chloride

With thionyl chloride; In benzene;

DOI:10.1016/S0040-4039(01)80505-0

Reference yield:

Carbamic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester (121666-42-0) → ((S)-1-Allyloxy-2,2,2-trichloro-ethyl)-carbamic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester (126442-14-6,126575-75-5)

Guidance literature:

Multi-step reaction with 3 steps

1: benzene / 20 h / Heating

2: thionyl chloride

With thionyl chloride; In benzene;

DOI:10.1016/S0040-4039(01)80505-0

Reference yield:

(2,2,2-Trichloro-1-hydroxy-ethyl)-carbamic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester → ((R)-1-Allyloxy-2,2,2-trichloro-ethyl)-carbamic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester (126442-14-6,126575-75-5)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride

With thionyl chloride;

DOI:10.1016/S0040-4039(01)80505-0

upstream raw materials:

allyl alcohol

Carbamic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester

Downstream raw materials:

(2S,4R)-4-Methyl-2-trichloromethyl-oxazolidine-3-carboxylic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester

(2R,4S)-4-Methyl-2-trichloromethyl-oxazolidine-3-carboxylic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester

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