C₂₁H₁₂F₅N₅O₂

Base Information

Chemical Name:C₂₁H₁₂F₅N₅O₂
CAS No.:1333931-21-7
Molecular Formula:C₂₁H₁₂F₅N₅O₂
Molecular Weight:461.351
Hs Code.:

C<sub>21</sub>H<sub>12</sub>F<sub>5</sub>N<sub>5</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₁₂F₅N₅O₂

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₂₁H₁₂F₅N₅O₂

There total 7 articles about C₂₁H₁₂F₅N₅O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5470-18-8,34515-82-7
2-Chloro-3-nitropyridine

: 1333931-21-7
C₂₁H₁₂F₅N₅O₂

Guidance literature:: Multi-step reaction with 6 steps

1: N-ethyl-N,N-diisopropylamine / 9 h / 20 - 60 °C

2: ethanol; ammonium chloride; zinc / 5 h / Reflux

3: hydrogenchloride / water / 15 h / Reflux

4: trichlorophosphate / acetonitrile / 3 h / Reflux

5: hydrazine hydrate / ethanol / 1 h / 60 °C

6: ethanol / 5 h / 60 °C

With hydrogenchloride; ethanol; ammonium chloride; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; zinc; trichlorophosphate; In ethanol; water; acetonitrile;
DOI:10.1016/j.cclet.2011.05.031

Reference yield:

: 1333931-08-0
3-nitro-N-(4-(trifluoromethoxy)phenyl)pyridin-2-amine

: 1333931-21-7
C₂₁H₁₂F₅N₅O₂

Guidance literature:: Multi-step reaction with 5 steps

1: ethanol; ammonium chloride; zinc / 5 h / Reflux

2: hydrogenchloride / water / 15 h / Reflux

3: trichlorophosphate / acetonitrile / 3 h / Reflux

4: hydrazine hydrate / ethanol / 1 h / 60 °C

5: ethanol / 5 h / 60 °C

With hydrogenchloride; ethanol; ammonium chloride; hydrazine hydrate; zinc; trichlorophosphate; In ethanol; water; acetonitrile;
DOI:10.1016/j.cclet.2011.05.031

Reference yield:

: 1038352-75-8
C₁₂H₁₀F₃N₃O

: 1333931-21-7
C₂₁H₁₂F₅N₅O₂

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / water / 15 h / Reflux

2: trichlorophosphate / acetonitrile / 3 h / Reflux

3: hydrazine hydrate / ethanol / 1 h / 60 °C

4: ethanol / 5 h / 60 °C

With hydrogenchloride; hydrazine hydrate; trichlorophosphate; In ethanol; water; acetonitrile;
DOI:10.1016/j.cclet.2011.05.031