(C₆H₅CNNH₂C₆H₅)Cr(CO)3

Base Information

Chemical Name:(C₆H₅CNNH₂C₆H₅)Cr(CO)3
CAS No.:170955-30-3
Molecular Formula:C₁₆H₁₂CrN₂O₃
Molecular Weight:332.279
Hs Code.:

(C<sub>6</sub>H<sub>5</sub>CNNH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)Cr(CO)3

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (C₆H₅CNNH₂C₆H₅)Cr(CO)3

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Technology Process of (C₆H₅CNNH₂C₆H₅)Cr(CO)3

There total 1 articles about (C₆H₅CNNH₂C₆H₅)Cr(CO)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 41371-94-2,14974-11-9,96647-88-0
tris(ammonia)chromium tricarbonyl

: 5350-57-2
benzophenone hydrazone

: 15228-27-0
pentacarbonyl(ammonia)chromium

: 170955-30-3
(C₆H₅CNNH₂C₆H₅)Cr(CO)3

: (C₆H₅)2CNNH₂*Cr*5CO=(C₆H₅)2CNNH₂*Cr(CO)5

Guidance literature:: In 1,4-dioxane; reflux (1 h, Ar-atmosphere), cooling; ppt. filtration off (silica gel), solvent removing, residue dissoln. in benzene, chromy. (silica gel/hexane-benzene); elem. anal.;
DOI:10.1007/BF00698519

Reference yield: 25.0%

: 170955-30-3
(C₆H₅CNNH₂C₆H₅)Cr(CO)3

: 99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0
fullerene-C₆₀

: (C₆H₅CN₂C₆H₅)Cr(CO)3*C₆₀=(C₆H₅CN₂C₆H₅)Cr(CO)3C₆₀

Guidance literature:: With manganese(IV) oxide; magnesium sulfate; In dichloromethane; byproducts: C60*C(C6H5)2; Mg- and Mn-compounds addn. to CH2Cl2-soln. of Cr-compd., stirring (room temperature, .apprx. 3 h), soln. filtration, solvent removing in vacuum (no heating), toluene soln. of the residue addn. to toluene soln. of fullerene, standing (72 h); silica gel addn., solvent removing (vacuum), dry residue placing to silica gel column, elution by heptane (C60), toluene-heptane (C60*CPh2, thenCr-product); elem. anal.;
DOI:10.1007/BF00698519