Technology Process of C33H28N2O2S2
There total 5 articles about C33H28N2O2S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
ethanol; water; toluene;
for 8h;
Inert atmosphere;
Reflux;
DOI:10.1016/j.dyepig.2011.08.005
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: acetic acid / benzene / Inert atmosphere
1.2: 4 h / Inert atmosphere; Reflux
1.3: Inert atmosphere
2.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; water; toluene / 8 h / Inert atmosphere; Reflux
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate; acetic acid;
In
ethanol; water; toluene; benzene;
2.1: Suzuki coupling;
DOI:10.1016/j.dyepig.2011.08.005
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: aluminum (III) chloride / carbon disulfide / Inert atmosphere
2.1: ammonium acetate; acetic acid / 1 h / Inert atmosphere; Reflux
2.2: Inert atmosphere; Reflux
2.3: Cooling; Inert atmosphere
3.1: acetic acid / benzene / Inert atmosphere
3.2: 4 h / Inert atmosphere; Reflux
3.3: Inert atmosphere
4.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; water; toluene / 8 h / Inert atmosphere; Reflux
With
aluminum (III) chloride; tetrakis(triphenylphosphine) palladium(0); ammonium acetate; potassium carbonate; acetic acid;
In
carbon disulfide; ethanol; water; toluene; benzene;
4.1: Suzuki coupling;
DOI:10.1016/j.dyepig.2011.08.005
