C₃₂H₃₇NO₄Si

Base Information

Chemical Name:C₃₂H₃₇NO₄Si
CAS No.:1256603-72-1
Molecular Formula:C₃₂H₃₇NO₄Si
Molecular Weight:527.736
Hs Code.:

C<sub>32</sub>H<sub>37</sub>NO<sub>4</sub>Si

Synonyms:

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Chemical Property of C₃₂H₃₇NO₄Si

Chemical Property:

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Technology Process of C₃₂H₃₇NO₄Si

There total 23 articles about C₃₂H₃₇NO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1256603-55-0
C₁₃H₁₉BrO₆

: 1256603-72-1
C₃₂H₃₇NO₄Si

Guidance literature:: Multi-step reaction with 17 steps

1.1: potassium carbonate / methanol / 1 h / 18 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; benzene / 18 °C / Inert atmosphere; Reflux

3.1: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / 18 h / 18 °C

4.1: potassium carbonate / methanol / 1 h / 18 °C

5.1: toluene / 168 h / Reflux

6.1: bromine / toluene / 18 h / 18 °C

6.2: 2 h

7.1: palladium 10% on activated carbon; hydrogen; potassium carbonate / methanol / 18 h / 18 °C

8.1: dmap / pyridine / 2 h / 18 °C

9.1: acetic acid / water / 20 h / 18 °C

10.1: dmap / dichloromethane / 1 h / 0 °C / Inert atmosphere

11.1: phosphorous acid trimethyl ester / toluene / 18 h / Reflux

12.1: potassium carbonate / methanol / 1 h / 18 °C

13.1: 1H-imidazole / dichloromethane / 18 h / 18 °C / Inert atmosphere

14.1: lithium triethylborohydride / tetrahydrofuran / 4 h / 18 °C / Inert atmosphere

15.1: Dess-Martin periodane / dichloromethane / 16 h / 18 °C

16.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 0.75 h / 95 °C

17.1: tetrahydrofuran; tetrachloromethane / 0.75 h / 95 °C

With 1H-imidazole; dmap; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2'-azobis(isobutyronitrile); di-isopropyl azodicarboxylate; palladium 10% on activated carbon; hydrogen; bromine; lithium triethylborohydride; sodium carbonate; potassium carbonate; Dess-Martin periodane; acetic acid; triphenylphosphine; phosphorous acid trimethyl ester; In tetrahydrofuran; pyridine; methanol; tetrachloromethane; dichloromethane; water; toluene; benzene; 2.1: Suzuki-Miyaura cross-coupling / 3.1: Mitsunobu reaction / 11.1: Corey-Winter olefination reaction;
DOI:10.1071/CH10201

Reference yield:

: 1256603-54-9
C₁₁H₁₅BrO₅

: 1256603-72-1
C₃₂H₃₇NO₄Si

Guidance literature:: Multi-step reaction with 18 steps

1.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 18 °C / Inert atmosphere

2.1: potassium carbonate / methanol / 1 h / 18 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; benzene / 18 °C / Inert atmosphere; Reflux

4.1: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / 18 h / 18 °C

5.1: potassium carbonate / methanol / 1 h / 18 °C

6.1: toluene / 168 h / Reflux

7.1: bromine / toluene / 18 h / 18 °C

7.2: 2 h

8.1: palladium 10% on activated carbon; hydrogen; potassium carbonate / methanol / 18 h / 18 °C

9.1: dmap / pyridine / 2 h / 18 °C

10.1: acetic acid / water / 20 h / 18 °C

11.1: dmap / dichloromethane / 1 h / 0 °C / Inert atmosphere

12.1: phosphorous acid trimethyl ester / toluene / 18 h / Reflux

13.1: potassium carbonate / methanol / 1 h / 18 °C

14.1: 1H-imidazole / dichloromethane / 18 h / 18 °C / Inert atmosphere

15.1: lithium triethylborohydride / tetrahydrofuran / 4 h / 18 °C / Inert atmosphere

16.1: Dess-Martin periodane / dichloromethane / 16 h / 18 °C

17.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 0.75 h / 95 °C

18.1: tetrahydrofuran; tetrachloromethane / 0.75 h / 95 °C

With 1H-imidazole; dmap; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2'-azobis(isobutyronitrile); di-isopropyl azodicarboxylate; palladium 10% on activated carbon; hydrogen; bromine; lithium triethylborohydride; sodium carbonate; potassium carbonate; Dess-Martin periodane; acetic acid; N-ethyl-N,N-diisopropylamine; triphenylphosphine; phosphorous acid trimethyl ester; In tetrahydrofuran; pyridine; methanol; tetrachloromethane; dichloromethane; water; toluene; benzene; 3.1: Suzuki-Miyaura cross-coupling / 4.1: Mitsunobu reaction / 12.1: Corey-Winter olefination reaction;
DOI:10.1071/CH10201

Reference yield:

: 130669-74-8
(1S,2S,5R,6R)-3-bromo-5,6-epoxy-1,2-O-isopropylidencyclohex-3-en-1,2-diol

: 1256603-72-1
C₃₂H₃₇NO₄Si

Guidance literature:: Multi-step reaction with 19 steps

1.1: phosphoric acid / 1 h / 18 °C

2.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 18 °C / Inert atmosphere

3.1: potassium carbonate / methanol / 1 h / 18 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; benzene / 18 °C / Inert atmosphere; Reflux

5.1: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / 18 h / 18 °C

6.1: potassium carbonate / methanol / 1 h / 18 °C

7.1: toluene / 168 h / Reflux

8.1: bromine / toluene / 18 h / 18 °C

8.2: 2 h

9.1: palladium 10% on activated carbon; hydrogen; potassium carbonate / methanol / 18 h / 18 °C

10.1: dmap / pyridine / 2 h / 18 °C

11.1: acetic acid / water / 20 h / 18 °C

12.1: dmap / dichloromethane / 1 h / 0 °C / Inert atmosphere

13.1: phosphorous acid trimethyl ester / toluene / 18 h / Reflux

14.1: potassium carbonate / methanol / 1 h / 18 °C

15.1: 1H-imidazole / dichloromethane / 18 h / 18 °C / Inert atmosphere

16.1: lithium triethylborohydride / tetrahydrofuran / 4 h / 18 °C / Inert atmosphere

17.1: Dess-Martin periodane / dichloromethane / 16 h / 18 °C

18.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 0.75 h / 95 °C

19.1: tetrahydrofuran; tetrachloromethane / 0.75 h / 95 °C

With 1H-imidazole; dmap; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2'-azobis(isobutyronitrile); di-isopropyl azodicarboxylate; phosphoric acid; palladium 10% on activated carbon; hydrogen; bromine; lithium triethylborohydride; sodium carbonate; potassium carbonate; Dess-Martin periodane; acetic acid; N-ethyl-N,N-diisopropylamine; triphenylphosphine; phosphorous acid trimethyl ester; In tetrahydrofuran; pyridine; methanol; tetrachloromethane; dichloromethane; water; toluene; benzene; 4.1: Suzuki-Miyaura cross-coupling / 5.1: Mitsunobu reaction / 13.1: Corey-Winter olefination reaction;
DOI:10.1071/CH10201