C₅₀H₄₆O₆P⁽¹⁺⁾*Br^(1-)

Base Information

Chemical Name:C₅₀H₄₆O₆P⁽¹⁺⁾*Br^(1-)
CAS No.:1415228-97-5
Molecular Formula:Br*C₅₀H₄₆O₆P
Molecular Weight:853.789
Hs Code.:

C<sub>50</sub>H<sub>46</sub>O<sub>6</sub>P<sup>(1+)</sup>*Br<sup>(1-)</sup>

Synonyms:

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Chemical Property of C₅₀H₄₆O₆P⁽¹⁺⁾*Br^(1-)

Chemical Property:

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Technology Process of C₅₀H₄₆O₆P⁽¹⁺⁾*Br^(1-)

There total 7 articles about C₅₀H₄₆O₆P⁽¹⁺⁾*Br^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1415228-88-4
C₃₅H₃₆O₉

: 1415228-97-5
C₅₀H₄₆O₆P⁽¹⁺⁾*Br^(1-)

Guidance literature:: Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / diethyl ether / 3 h / 0 °C

2: water / 4 h / 20 °C / Acidic conditions

3: carbon tetrabromide; triphenylphosphine / benzene / 17 h / Reflux

4: acetonitrile / 24 h / Reflux

With lithium aluminium tetrahydride; carbon tetrabromide; triphenylphosphine; In diethyl ether; water; acetonitrile; benzene;
DOI:10.1016/j.bmcl.2012.10.052

Reference yield:

: 1415228-93-1
C₃₂H₃₂O₇

: 1415228-97-5
C₅₀H₄₆O₆P⁽¹⁺⁾*Br^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1: carbon tetrabromide; triphenylphosphine / benzene / 17 h / Reflux

2: acetonitrile / 24 h / Reflux

With carbon tetrabromide; triphenylphosphine; In acetonitrile; benzene;
DOI:10.1016/j.bmcl.2012.10.052

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 1415228-97-5
C₅₀H₄₆O₆P⁽¹⁺⁾*Br^(1-)

Guidance literature:: Multi-step reaction with 7 steps

1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 120 °C

2: potassium carbonate; 18-crown-6 ether / dichloromethane / 15 h / Reflux

3: palladium 10% on activated carbon; hydrogen; triethylamine / ethyl acetate / 5 h / 20 °C

4: lithium aluminium tetrahydride / diethyl ether / 3 h / 0 °C

5: water / 4 h / 20 °C / Acidic conditions

6: carbon tetrabromide; triphenylphosphine / benzene / 17 h / Reflux

7: acetonitrile / 24 h / Reflux

With lithium aluminium tetrahydride; 18-crown-6 ether; carbon tetrabromide; palladium 10% on activated carbon; hydrogen; potassium carbonate; triethylamine; triphenylphosphine; In diethyl ether; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; benzene; 2: |Wittig Olefination;
DOI:10.1016/j.bmcl.2012.10.052