methyl 2,3,4-tri-O-benzoyl-6-O-amino-α-D-glucopyranoside hydrochloride

Base Information

Chemical Name:methyl 2,3,4-tri-O-benzoyl-6-O-amino-α-D-glucopyranoside hydrochloride
CAS No.:1353742-12-7
Molecular Formula:C₂₈H₂₇NO₉*ClH
Molecular Weight:557.985
Hs Code.:

Synonyms:

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Chemical Property of methyl 2,3,4-tri-O-benzoyl-6-O-amino-α-D-glucopyranoside hydrochloride

Chemical Property:

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Technology Process of methyl 2,3,4-tri-O-benzoyl-6-O-amino-α-D-glucopyranoside hydrochloride

There total 3 articles about methyl 2,3,4-tri-O-benzoyl-6-O-amino-α-D-glucopyranoside hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353844-15-1
methyl 2,3,4-tri-O-benzoyl-6-O-amino-α-D-glucopyranoside

: 1353742-12-7
methyl 2,3,4-tri-O-benzoyl-6-O-amino-α-D-glucopyranoside hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; tert-butyl methyl ether; Inert atmosphere;
DOI:10.1021/ol203213f

Reference yield:

: 34234-44-1
methyl 2,3,4-tri-O-benzoylglucopyranoside

: 1353742-12-7
methyl 2,3,4-tri-O-benzoyl-6-O-amino-α-D-glucopyranoside hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine / tetrahydrofuran / 0.17 h / Inert atmosphere

1.2: 18 h / 0 - 20 °C / Inert atmosphere

2.1: hydrazine hydrate / methanol; dichloromethane / 5 h / 20 °C / Inert atmosphere

3.1: hydrogenchloride / diethyl ether; tert-butyl methyl ether / Inert atmosphere

With hydrogenchloride; hydrazine hydrate; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; tert-butyl methyl ether;
DOI:10.1021/ol203213f

Reference yield:

: 1353742-11-6
methyl 2,3,4-tri-O-benzoyl-6-O-(1,3-dioxoisoindolin-2-yl)-α-D-glucopyranoside

: 1353742-12-7
methyl 2,3,4-tri-O-benzoyl-6-O-amino-α-D-glucopyranoside hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol; dichloromethane / 5 h / 20 °C / Inert atmosphere

2: hydrogenchloride / diethyl ether; tert-butyl methyl ether / Inert atmosphere

With hydrogenchloride; hydrazine hydrate; In methanol; diethyl ether; dichloromethane; tert-butyl methyl ether;
DOI:10.1021/ol203213f