methyl 2,3,4-tri-O-benzoyl-6-O-(1,3-dioxoisoindolin-2-yl)-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2,3,4-tri-O-benzoyl-6-O-(1,3-dioxoisoindolin-2-yl)-α-D-glucopyranoside
CAS No.:1353742-11-6
Molecular Formula:C₃₆H₂₉NO₁₁
Molecular Weight:651.626
Hs Code.:

Synonyms:methyl 2,3,4-tri-O-benzoyl-6-O-(1,3-dioxoisoindolin-2-yl)-α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,3,4-tri-O-benzoyl-6-O-(1,3-dioxoisoindolin-2-yl)-α-D-glucopyranoside

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Technology Process of methyl 2,3,4-tri-O-benzoyl-6-O-(1,3-dioxoisoindolin-2-yl)-α-D-glucopyranoside

There total 1 articles about methyl 2,3,4-tri-O-benzoyl-6-O-(1,3-dioxoisoindolin-2-yl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 34234-44-1
methyl 2,3,4-tri-O-benzoylglucopyranoside

: 524-38-9
N-hydroxyphthalimide

: 1353742-11-6
methyl 2,3,4-tri-O-benzoyl-6-O-(1,3-dioxoisoindolin-2-yl)-α-D-glucopyranoside

Guidance literature:: methyl 2,3,4-tri-O-benzoylglucopyranoside; N-hydroxyphthalimide; With triphenylphosphine; In tetrahydrofuran; for 0.166667h; Inert atmosphere;

With di-isopropyl azodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/ol203213f

Reference yield:

: 1353742-11-6
methyl 2,3,4-tri-O-benzoyl-6-O-(1,3-dioxoisoindolin-2-yl)-α-D-glucopyranoside

: 1353844-15-1
methyl 2,3,4-tri-O-benzoyl-6-O-amino-α-D-glucopyranoside

Guidance literature:: methyl 2,3,4-tri-O-benzoyl-6-O-(1,3-dioxoisoindolin-2-yl)-α-D-glucopyranoside; With hydrazine hydrate; In methanol; dichloromethane; at 20 ℃; for 5h; Inert atmosphere;

In tert-butyl methyl ether;
DOI:10.1021/ol203213f

Reference yield:

: 1353742-11-6
methyl 2,3,4-tri-O-benzoyl-6-O-(1,3-dioxoisoindolin-2-yl)-α-D-glucopyranoside

: 1353742-12-7
methyl 2,3,4-tri-O-benzoyl-6-O-amino-α-D-glucopyranoside hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol; dichloromethane / 5 h / 20 °C / Inert atmosphere

2: hydrogenchloride / diethyl ether; tert-butyl methyl ether / Inert atmosphere

With hydrogenchloride; hydrazine hydrate; In methanol; diethyl ether; dichloromethane; tert-butyl methyl ether;
DOI:10.1021/ol203213f