H₄H(2,2)TIAM

Base Information

Chemical Name:H₄H(2,2)TIAM
CAS No.:872705-83-4
Molecular Formula:C₅₄H₆₈N₁₄O₁₆
Molecular Weight:1169.22
Hs Code.:

Synonyms:

Suppliers and Price of H₄H(2,2)TIAM

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of H₄H(2,2)TIAM

Chemical Property:

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Technology Process of H₄H(2,2)TIAM

There total 7 articles about H₄H(2,2)TIAM which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 872705-74-3
1-methoxy-2,4,6-benzenetricarbonyl trichloride

: 872705-83-4
H₄H(2,2)TIAM

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dichloromethane

2: dichloromethane; water; isopropyl alcohol / 48 h

3: dichloromethane; water; isopropyl alcohol / 48 h

4: dichloromethane

5: boron tribromide / dichloromethane / 64 h / Inert atmosphere

With boron tribromide; triethylamine; In dichloromethane; water; isopropyl alcohol;
DOI:10.1002/anie.201106748

Reference yield:

: 17445-86-2
1-methoxybenzene-2,4,6-tricarboxylic acid

: 872705-83-4
H₄H(2,2)TIAM

Guidance literature:: Multi-step reaction with 6 steps

1: thionyl chloride; N,N-dimethyl-formamide / 1,4-dioxane / Reflux; Inert atmosphere

2: triethylamine / dichloromethane

3: dichloromethane; water; isopropyl alcohol / 48 h

4: dichloromethane; water; isopropyl alcohol / 48 h

5: dichloromethane

6: boron tribromide / dichloromethane / 64 h / Inert atmosphere

With thionyl chloride; boron tribromide; triethylamine; N,N-dimethyl-formamide; In 1,4-dioxane; dichloromethane; water; isopropyl alcohol;
DOI:10.1002/anie.201106748

Reference yield:

: 91-04-3
2,6-bis(hydroxymethyl)-4-methylphenol

: 872705-83-4
H₄H(2,2)TIAM

Guidance literature:: Multi-step reaction with 8 steps

1: sodium hydroxide / water

2: potassium permanganate; sodium hydroxide / water / 20 - 90 °C

3: thionyl chloride; N,N-dimethyl-formamide / 1,4-dioxane / Reflux; Inert atmosphere

4: triethylamine / dichloromethane

5: dichloromethane; water; isopropyl alcohol / 48 h

6: dichloromethane; water; isopropyl alcohol / 48 h

7: dichloromethane

8: boron tribromide / dichloromethane / 64 h / Inert atmosphere

With potassium permanganate; thionyl chloride; boron tribromide; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In 1,4-dioxane; dichloromethane; water; isopropyl alcohol;
DOI:10.1002/anie.201106748