Technology Process of C31H33F3N4O10S
There total 5 articles about C31H33F3N4O10S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: methanesulfonyl chloride; triethylamine / dichloromethane / 0 - 20 °C
2: caesium carbonate; potassium iodide / acetonitrile / 1 h / Reflux
With
caesium carbonate; methanesulfonyl chloride; triethylamine; potassium iodide;
In
dichloromethane; acetonitrile;
DOI:10.1021/ol5012218
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hexamethylenetetramine / water / 125 °C
2: sodium tetrahydroborate / methanol / 0 - 20 °C
3: potassium carbonate / N,N-dimethyl-formamide / 1 h / 75 °C
4: methanesulfonyl chloride; triethylamine / dichloromethane / 0 - 20 °C
5: caesium carbonate; potassium iodide / acetonitrile / 1 h / Reflux
With
sodium tetrahydroborate; hexamethylenetetramine; potassium carbonate; caesium carbonate; methanesulfonyl chloride; triethylamine; potassium iodide;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol5012218
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium tetrahydroborate / methanol / 0 - 20 °C
2: potassium carbonate / N,N-dimethyl-formamide / 1 h / 75 °C
3: methanesulfonyl chloride; triethylamine / dichloromethane / 0 - 20 °C
4: caesium carbonate; potassium iodide / acetonitrile / 1 h / Reflux
With
sodium tetrahydroborate; potassium carbonate; caesium carbonate; methanesulfonyl chloride; triethylamine; potassium iodide;
In
methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol5012218