C₅₂H₄₆Cl₁₂Si₄

Base Information

Chemical Name:C₅₂H₄₆Cl₁₂Si₄
CAS No.:1281831-58-0
Molecular Formula:C₅₂H₄₆Cl₁₂Si₄
Molecular Weight:1208.72
Hs Code.:

C<sub>52</sub>H<sub>46</sub>Cl<sub>12</sub>Si<sub>4</sub>

Synonyms:

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Chemical Property of C₅₂H₄₆Cl₁₂Si₄

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Technology Process of C₅₂H₄₆Cl₁₂Si₄

There total 3 articles about C₅₂H₄₆Cl₁₂Si₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1281831-57-9
1,3,6,8-tetrakis(4-allylphenyl)pyrene

: 1281831-58-0
C₅₂H₄₆Cl₁₂Si₄

Guidance literature:: With Speier's catalyst; trichlorosilane; In benzene; at 0 - 40 ℃; regioselective reaction; Inert atmosphere; Darkness;
DOI:10.1246/cl.2012.316

Reference yield:

: 624-38-4,1032416-46-8
para-diiodobenzene

: 1281831-58-0
C₅₂H₄₆Cl₁₂Si₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: isopropylmagnesium chloride / tetrahydrofuran / 8 h / -30 °C / Inert atmosphere

1.2: -30 - 20 °C / Inert atmosphere

2.1: isopropylmagnesium chloride / tetrahydrofuran / 8 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,4-dioxane; water / 72 h / 90 °C / Inert atmosphere

4.1: Speier's catalyst; trichlorosilane / benzene / 0 - 40 °C / Inert atmosphere; Darkness

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; Speier's catalyst; trichlorosilane; isopropylmagnesium chloride; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; water; benzene; 3.1: Suzuki coupling;
DOI:10.1246/cl.2012.316

Reference yield:

: 1-allyl-4-iodobenzene

: 1281831-58-0
C₅₂H₄₆Cl₁₂Si₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: isopropylmagnesium chloride / tetrahydrofuran / 8 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,4-dioxane; water / 72 h / 90 °C / Inert atmosphere

3.1: Speier's catalyst; trichlorosilane / benzene / 0 - 40 °C / Inert atmosphere; Darkness

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; Speier's catalyst; trichlorosilane; isopropylmagnesium chloride; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; water; benzene; 2.1: Suzuki coupling;
DOI:10.1246/cl.2012.316