Mo₂Cp₂{(μ-C(Ph)CO)}(μ-PCy₂)(CO)₂

Base Information

Chemical Name:Mo₂Cp₂{(μ-C(Ph)CO)}(μ-PCy₂)(CO)₂
CAS No.:1208114-70-8
Molecular Formula:C₃₂H₃₇Mo₂O₃P
Molecular Weight:692.498
Hs Code.:

Mo<sub>2</sub>Cp<sub>2</sub>{(μ-C(Ph)CO)}(μ-PCy<sub>2</sub>)(CO)<sub>2</sub>

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Chemical Property of Mo₂Cp₂{(μ-C(Ph)CO)}(μ-PCy₂)(CO)₂

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Technology Process of Mo₂Cp₂{(μ-C(Ph)CO)}(μ-PCy₂)(CO)₂

There total 2 articles about Mo₂Cp₂{(μ-C(Ph)CO)}(μ-PCy₂)(CO)₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 201230-82-2
carbon monoxide

: 1208114-69-5
[Mo₂(η⁵-C₅H₅)₂(μ-CPh)(μ-PCy₂)(μ-CO)]

: 1208114-70-8
Mo₂Cp₂{(μ-C(Ph)CO)}(μ-PCy₂)(CO)₂

Guidance literature:: In toluene; under N2; toluene soln. of Mo complex cooled to 77 K; evacuated under vac.; CO introduced; closed; warmed to room temp.; stirred for 40 h; solvent removed under vac.; column chromd. (alumina, CH2Cl2-petroleum ether 1:6) at 288 K; green fraction collected; solvent removed under vac.;elem. anal.;
DOI:10.1021/om1011819

Reference yield:

: 201230-82-2
carbon monoxide

: 1286281-95-5
[Mo2(η⁵-C₅H₅)₂(μ-CPh)(μ-PCy₂)(CO)₂]

: 1208114-70-8
Mo₂Cp₂{(μ-C(Ph)CO)}(μ-PCy₂)(CO)₂

Guidance literature:: In not given; High Pressure; under N2; Mo complex reacted with CO (4 bar) at broom temp. for ca. 4 h;
DOI:10.1021/om1011819

Reference yield: 89.0%

: 1208114-70-8
Mo₂Cp₂{(μ-C(Ph)CO)}(μ-PCy₂)(CO)₂

: 908093-98-1
diazodiphenylmethane

: 1313211-16-3
[Mo₂Cp₂{μ-κ¹:η²-C(Ph)CO}(μ-PCy₂)(CO)(κ¹-N₂CPh₂)]

Guidance literature:: In diethyl ether; dichloromethane; at 20 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.organomet.6b00552