C₂₄H₁₈N₂O₈S₄

Base Information

• Chemical Name: C₂₄H₁₈N₂O₈S₄
• CAS No.: 1403384-89-3
• Molecular Formula: C₂₄H₁₈N₂O₈S₄
• Molecular Weight: 590.68
• Mol file: 1403384-89-3.mol

Synonyms:

Chemical Property of C₂₄H₁₈N₂O₈S₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₁₈N₂O₈S₄

There total 4 articles about C₂₄H₁₈N₂O₈S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

disodium 2,6-naphthalenedisulfonate (1655-45-4) → C24H18N2O8S4 (1403384-89-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: chlorosulfonic acid / chloroform / 3 h / 60 °C / Inert atmosphere; Cooling with ice

2.1: pyridine / 3 h / Reflux

3.1: potassium hydroxide / ethanol / 0.67 h / Inert atmosphere; Reflux

3.2: Inert atmosphere; Cooling with ice

With pyridine; chlorosulfonic acid; potassium hydroxide; In ethanol; chloroform;

DOI:10.1021/ol302260n

Reference yield:

C32H32N4O10S4 (1403385-04-5) → C24H18N2O8S4 (1403384-89-3)

Guidance literature:

C₃₂H₃₂N₄O₁₀S₄; With potassium hydroxide; In ethanol; for 0.666667h; Inert atmosphere; Reflux;

With hydrogenchloride; In ethanol; water; Inert atmosphere; Cooling with ice;

DOI:10.1021/ol302260n

Reference yield:

methyl 2-hydroxy-5-nitrobenzoate (17302-46-4) → C24H18N2O8S4 (1403384-89-3)

Guidance literature:

Multi-step reaction with 5 steps

1.1: 1,4-diaza-bicyclo[2.2.2]octane / N,N-dimethyl-formamide / 48 h / 20 °C

2.1: 0.33 h / 150 °C

3.1: acetic acid; zinc / 0.75 h / Reflux

4.1: pyridine / 3 h / Reflux

5.1: potassium hydroxide / ethanol / 0.67 h / Inert atmosphere; Reflux

5.2: Inert atmosphere; Cooling with ice

With pyridine; 1,4-diaza-bicyclo[2.2.2]octane; acetic acid; potassium hydroxide; zinc; In ethanol; N,N-dimethyl-formamide;

DOI:10.1021/ol302260n

upstream raw materials:

disodium 2,6-naphthalenedisulfonate

C₃₂H₃₂N₄O₁₀S₄

methyl 2-hydroxy-5-nitrobenzoate

2-dimethylthiocarbamoyloxy-5-nitrobenzoic acid methyl ester