Acetic acid 2-{24-[(E)-2-acetylamino-ethoxyimino]-3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21-hexaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.0^6,10]hexacos-15-ylcarbamoyl}-pyridin-3-yl ester

Base Information

• Chemical Name: Acetic acid 2-{24-[(E)-2-acetylamino-ethoxyimino]-3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21-hexaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.0^6,10]hexacos-15-ylcarbamoyl}-pyridin-3-yl ester
• CAS No.: 129412-75-5
• Molecular Formula: C₄₉H₅₉N₉O₁₂
• Molecular Weight: 966.061

Synonyms:

Chemical Property of Acetic acid 2-{24-[(E)-2-acetylamino-ethoxyimino]-3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21-hexaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.0^6,10]hexacos-15-ylcarbamoyl}-pyridin-3-yl ester

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Technology Process of Acetic acid 2-{24-[(E)-2-acetylamino-ethoxyimino]-3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21-hexaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.0^6,10]hexacos-15-ylcarbamoyl}-pyridin-3-yl ester

There total 2 articles about Acetic acid 2-{24-[(E)-2-acetylamino-ethoxyimino]-3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21-hexaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.0^6,10]hexacos-15-ylcarbamoyl}-pyridin-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

virginiamycin S aminoethyloxime (129412-73-3) + acetyl chloride (75-36-5) → Acetic acid 2-{24-[(E)-2-acetylamino-ethoxyimino]-3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21-hexaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.06,10]hexacos-15-ylcarbamoyl}-pyridin-3-yl ester (129412-75-5,129446-54-4)

Guidance literature:

With TEA; In dichloromethane; for 1h;

Reference yield:

virginiamycin S1 (668-72-4,23152-29-6,117603-96-0) → Acetic acid 2-{24-[(E)-2-acetylamino-ethoxyimino]-3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21-hexaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.06,10]hexacos-15-ylcarbamoyl}-pyridin-3-yl ester (129412-75-5,129446-54-4)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / ethanol / 2 h

2: 73 percent / Tea / CH₂Cl₂ / 1 h

With pyridine; TEA; In ethanol; dichloromethane;

upstream raw materials:

virginiamycin S aminoethyloxime

acetyl chloride

virginiamycin S₁

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