(R)-Methoxy-phenyl-acetic acid (S)-2-(6,8-dimethoxy-1-oxo-1H-isochromen-3-yl)-1-methyl-ethyl ester

Base Information

Chemical Name:(R)-Methoxy-phenyl-acetic acid (S)-2-(6,8-dimethoxy-1-oxo-1H-isochromen-3-yl)-1-methyl-ethyl ester
CAS No.:123297-83-6
Molecular Formula:C₂₃H₂₄O₇
Molecular Weight:412.439
Hs Code.:

Synonyms:

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Chemical Property of (R)-Methoxy-phenyl-acetic acid (S)-2-(6,8-dimethoxy-1-oxo-1H-isochromen-3-yl)-1-methyl-ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of (R)-Methoxy-phenyl-acetic acid (S)-2-(6,8-dimethoxy-1-oxo-1H-isochromen-3-yl)-1-methyl-ethyl ester

There total 7 articles about (R)-Methoxy-phenyl-acetic acid (S)-2-(6,8-dimethoxy-1-oxo-1H-isochromen-3-yl)-1-methyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5859-68-7
[(3,5-dimethoxyphenyl)methyl]propanedioic acid diethyl ester

: 123297-83-6
(R)-Methoxy-phenyl-acetic acid (S)-2-(6,8-dimethoxy-1-oxo-1H-isochromen-3-yl)-1-methyl-ethyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 80.6 percent / sodium ethoxyde / ethanol / Heating

2: 97.6 percent / potassium hydroxide, 18-crown-6 / H₂O; dioxane

3: 89.1 percent / trifluoroacetic anhydride

4: 1.) mercuric acetate; 2.) sodium borohydride / 1.) water, THF, r.t.

6: 1.) ozon; 2.) dimethyl sulfide / 1.) ethyl acetate, -70 deg C

With potassium hydroxide; sodium tetrahydroborate; 18-crown-6 ether; dimethylsulfide; mercury(II) diacetate; sodium ethanolate; ozone; trifluoroacetic anhydride; In 1,4-dioxane; ethanol; water;

Reference yield:

: 123297-77-8
2-Allyl-2-(3,5-dimethoxy-benzyl)-malonic acid diethyl ester

: 123297-83-6
(R)-Methoxy-phenyl-acetic acid (S)-2-(6,8-dimethoxy-1-oxo-1H-isochromen-3-yl)-1-methyl-ethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 97.6 percent / potassium hydroxide, 18-crown-6 / H₂O; dioxane

2: 89.1 percent / trifluoroacetic anhydride

3: 1.) mercuric acetate; 2.) sodium borohydride / 1.) water, THF, r.t.

5: 1.) ozon; 2.) dimethyl sulfide / 1.) ethyl acetate, -70 deg C

With potassium hydroxide; sodium tetrahydroborate; 18-crown-6 ether; dimethylsulfide; mercury(II) diacetate; ozone; trifluoroacetic anhydride; In 1,4-dioxane; water;

Reference yield:

: 123297-79-0
2-Allyl-5,7-dimethoxy-indan-1-one

: 123297-83-6
(R)-Methoxy-phenyl-acetic acid (S)-2-(6,8-dimethoxy-1-oxo-1H-isochromen-3-yl)-1-methyl-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) mercuric acetate; 2.) sodium borohydride / 1.) water, THF, r.t.

3: 1.) ozon; 2.) dimethyl sulfide / 1.) ethyl acetate, -70 deg C

With sodium tetrahydroborate; dimethylsulfide; mercury(II) diacetate; ozone;