Carbamic acid, diethyl-, 3-methyl-1,3-butadienyl ester, (E)-

Base Information

• Chemical Name: Carbamic acid, diethyl-, 3-methyl-1,3-butadienyl ester, (E)-
• CAS No.: 128728-58-5
• Molecular Formula: C₁₀H₁₇NO₂
• Molecular Weight: 183.25
• Mol file: 128728-58-5.mol

Synonyms:

Chemical Property of Carbamic acid, diethyl-, 3-methyl-1,3-butadienyl ester, (E)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Carbamic acid, diethyl-, 3-methyl-1,3-butadienyl ester, (E)-

There total 1 articles about Carbamic acid, diethyl-, 3-methyl-1,3-butadienyl ester, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3-dimethyl acrylaldehyde (107-86-8) + N,N-diethylcarbamyl chloride (88-10-8) → tert-butyl N,N-diethylcarbamate (51170-54-8) + Diethyl-carbamic acid (Z)-3-methyl-buta-1,3-dienyl ester (128728-59-6) + Diethyl-carbamic acid (E)-3-methyl-buta-1,3-dienyl ester (128728-58-5)

Guidance literature:

With potassium tert-butylate; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1) THF, -78 deg C 2) -78 deg C -> room temperature;

DOI:10.1016/S0040-4039(00)88817-6

upstream raw materials:

3,3-dimethyl acrylaldehyde

N,N-diethylcarbamyl chloride

Refernces