tert-butyl N,N-diethylcarbamate

Base Information

• Chemical Name: tert-butyl N,N-diethylcarbamate
• CAS No.: 51170-54-8
• Molecular Formula: C₉H₁₉NO₂
• Molecular Weight: 173.255
• Hs Code.: 2924297099
• Mol file: 51170-54-8.mol

Synonyms:tert-butyl N,N-diethylcarbamate

Chemical Property of tert-butyl N,N-diethylcarbamate

Chemical Property:

• Boiling Point: 28.4 °C(Press: 3 Torr)
• Density: 0.922±0.06 g/cm3(Predicted)

Purity/Quality:

97% ^*data from raw suppliers

tert-Butyldiethylcarbamate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tert-butyl N,N-diethylcarbamate

There total 11 articles about tert-butyl N,N-diethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

di-tert-butyl dicarbonate (24424-99-5) + diethylamine (109-89-7) → tert-butyl N,N-diethylcarbamate (51170-54-8)

Guidance literature:

With phenylsulfonic acid supported on mesoporous silica SBA-15; In neat (no solvent); at 20 ℃; for 0.0833333h; Green chemistry;

DOI:10.1007/s11164-015-2096-0

Reference yield: 94.0%

tert-butyl pyridin-2-yl carbonate (89985-91-1) + diethylamine (109-89-7) → tert-butyl N,N-diethylcarbamate (51170-54-8)

Guidance literature:

In dichloromethane; for 1.5h; Ambient temperature;

DOI:10.1246/bcsj.58.3570

Reference yield: 90.0%

diethylamine (109-89-7) + tert-butyl 1H-imidazole-1-carboxylate (49761-82-2) → tert-butyl N,N-diethylcarbamate (51170-54-8)

Guidance literature:

With Imidazole hydrochloride; In water; at 20 ℃; for 0.166667h;

DOI:10.1016/j.tetlet.2012.01.125

upstream raw materials:

trans-Crotonaldehyde

N,N-diethylcarbamyl chloride

3,3-dimethyl acrylaldehyde

t-butyl bromide

Downstream raw materials:

carbon dioxide

diethylamine

isobutene

tert-butyl ethyl(1-(pyridin-3-yl)ethyl)carbamate