Technology Process of C23H27F4N3O3S
There total 4 articles about C23H27F4N3O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate;
In
ethanol; toluene;
at 100 ℃;
for 1h;
Microwave irradiation;
DOI:10.1016/j.bmcl.2014.05.074
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dimethylsulfide borane complex / tetrahydrofuran
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / acetonitrile
3: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene; ethanol / 1 h / 100 °C / Microwave irradiation
With
tetrakis(triphenylphosphine) palladium(0); dimethylsulfide borane complex; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
tetrahydrofuran; ethanol; toluene; acetonitrile;
3: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2014.05.074
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / acetonitrile
2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene; ethanol / 1 h / 100 °C / Microwave irradiation
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
ethanol; toluene; acetonitrile;
2: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2014.05.074
