2--2-(p-dimethylaminophenyl)-7,8-benzo-1,3,6,9-tetraoxa-2-phosphacycloundecane

Base Information

Chemical Name:2--2-(p-dimethylaminophenyl)-7,8-benzo-1,3,6,9-tetraoxa-2-phosphacycloundecane
CAS No.:134296-50-7
Molecular Formula:C₂₅H₂₆F₃N₂O₆PS
Molecular Weight:570.526
Hs Code.:

2-<p-(Trifluoromethylsulfonyl)phenylimino>-2-(p-dimethylaminophenyl)-7,8-benzo-1,3,6,9-tetraoxa-2-phosphacycloundecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2--2-(p-dimethylaminophenyl)-7,8-benzo-1,3,6,9-tetraoxa-2-phosphacycloundecane

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Technology Process of 2--2-(p-dimethylaminophenyl)-7,8-benzo-1,3,6,9-tetraoxa-2-phosphacycloundecane

There total 4 articles about 2--2-(p-dimethylaminophenyl)-7,8-benzo-1,3,6,9-tetraoxa-2-phosphacycloundecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 31641-76-6
1-azido-4-(trifluoromethanesulfonyl)benzene

: 134284-19-8
2-(p-Dimethylaminophenyl)-7,8-benzo-1,3,6,9-tetraoxa-2-phosphacycloundecane

: 134296-50-7
2--2-(p-dimethylaminophenyl)-7,8-benzo-1,3,6,9-tetraoxa-2-phosphacycloundecane

Guidance literature:: In benzene; at 70 ℃; for 5h;

Reference yield:

: 10234-40-9
2,2'-(1,2-phenylenedioxy)diethanol

: 134296-50-7
2--2-(p-dimethylaminophenyl)-7,8-benzo-1,3,6,9-tetraoxa-2-phosphacycloundecane

Guidance literature:: Multi-step reaction with 2 steps

1: NEt₃ / benzene / 0.5 h / 10 - 15 °C

2: 19 percent / benzene / 5 h / 70 °C

With triethylamine; In benzene;

Reference yield:

: 29972-74-5
(4-dimethylamino-phenyl)-phosphonous acid dichloride

: 134296-50-7
2--2-(p-dimethylaminophenyl)-7,8-benzo-1,3,6,9-tetraoxa-2-phosphacycloundecane

Guidance literature:: Multi-step reaction with 2 steps

1: NEt₃ / benzene / 0.5 h / 10 - 15 °C

2: 19 percent / benzene / 5 h / 70 °C

With triethylamine; In benzene;