Technology Process of 7,8-Dihydro-6H-1,3-dioxolo[4,5-g][1]benzopyran-6-acetic acid
There total 3 articles about 7,8-Dihydro-6H-1,3-dioxolo[4,5-g][1]benzopyran-6-acetic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium permanganate; sodium periodate; potassium carbonate;
In
water; tert-butyl alcohol;
at 20 ℃;
for 3h;
DOI:10.1016/j.tetlet.2010.10.159
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trifluoroacetic acid / 6 h / 70 °C
2: triethylsilane; indium tribromide / toluene / 2 h / 70 °C
3: sodium periodate; potassium permanganate; potassium carbonate / water; tert-butyl alcohol / 3 h / 20 °C
With
triethylsilane; potassium permanganate; sodium periodate; indium tribromide; potassium carbonate; trifluoroacetic acid;
In
water; toluene; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2010.10.159
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylsilane; indium tribromide / toluene / 2 h / 70 °C
2: sodium periodate; potassium permanganate; potassium carbonate / water; tert-butyl alcohol / 3 h / 20 °C
With
triethylsilane; potassium permanganate; sodium periodate; indium tribromide; potassium carbonate;
In
water; toluene; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2010.10.159
