Sodium; 6-{2-[(E)-methoxyimino]-2-[2-(4-nitro-benzyloxycarbonylamino)-thiazol-4-yl]-acetylamino}-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

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Chemical Name:Sodium; 6-{2-[(E)-methoxyimino]-2-[2-(4-nitro-benzyloxycarbonylamino)-thiazol-4-yl]-acetylamino}-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate
CAS No.:85208-09-9
Molecular Formula:C₂₂H₂₁N₆O₉S₂*Na
Molecular Weight:600.565
Hs Code.:

Sodium; 6-{2-[(E)-methoxyimino]-2-[2-(4-nitro-benzyloxycarbonylamino)-thiazol-4-yl]-acetylamino}-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

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Chemical Property of Sodium; 6-{2-[(E)-methoxyimino]-2-[2-(4-nitro-benzyloxycarbonylamino)-thiazol-4-yl]-acetylamino}-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

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Technology Process of Sodium; 6-{2-[(E)-methoxyimino]-2-[2-(4-nitro-benzyloxycarbonylamino)-thiazol-4-yl]-acetylamino}-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

There total 5 articles about Sodium; 6-{2-[(E)-methoxyimino]-2-[2-(4-nitro-benzyloxycarbonylamino)-thiazol-4-yl]-acetylamino}-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81103-23-3
(E)-α-methoxyimino-α-<2-(4-nitrobenzyloxycarbonylamino)thiazol-4-yl>acetic acid

: 85208-09-9
Sodium; 6-{2-[(E)-methoxyimino]-2-[2-(4-nitro-benzyloxycarbonylamino)-thiazol-4-yl]-acetylamino}-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.21 g / PCl₅ / CH₂Cl₂ / 1 h / Ambient temperature

2: 1.) Et₃N, 2.) sodium 2-ethylhexanoate / 1.) CH₂Cl₂, pH=8-9, 1 h, 2.) methyl isobutyl ketone

With phosphorus pentachloride; triethylamine; sodium 2-ethylhexanoic acid; In dichloromethane;

Reference yield:

: 92592-07-9
ethyl (E)-α-methoxyimino-α-<3-(4-nitrobenzyloxycarbonyl)-2-(4-nitrobenzyloxycarbonylimino)-2,3-dihydrothiazol-4-yl>acetate

: 85208-09-9
Sodium; 6-{2-[(E)-methoxyimino]-2-[2-(4-nitro-benzyloxycarbonylamino)-thiazol-4-yl]-acetylamino}-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / KOH, H₂O / ethanol / 5 h / Ambient temperature

2: 1.21 g / PCl₅ / CH₂Cl₂ / 1 h / Ambient temperature

3: 1.) Et₃N, 2.) sodium 2-ethylhexanoate / 1.) CH₂Cl₂, pH=8-9, 1 h, 2.) methyl isobutyl ketone

With potassium hydroxide; phosphorus pentachloride; water; triethylamine; sodium 2-ethylhexanoic acid; In ethanol; dichloromethane;

Reference yield:

: 65052-66-6
2-(2-aminothiazol-4-yl)-2-methoxyiminoacetic acid-S-ethyl ester

: 85208-09-9
Sodium; 6-{2-[(E)-methoxyimino]-2-[2-(4-nitro-benzyloxycarbonylamino)-thiazol-4-yl]-acetylamino}-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 47 percent / aq.sodium hydrogen carbonate / CH₂Cl₂ / 2 h

2: 88 percent / KOH, H₂O / ethanol / 5 h / Ambient temperature

3: 1.21 g / PCl₅ / CH₂Cl₂ / 1 h / Ambient temperature

4: 1.) Et₃N, 2.) sodium 2-ethylhexanoate / 1.) CH₂Cl₂, pH=8-9, 1 h, 2.) methyl isobutyl ketone

With potassium hydroxide; phosphorus pentachloride; water; sodium hydrogencarbonate; triethylamine; sodium 2-ethylhexanoic acid; In ethanol; dichloromethane;