2-(Et-thio)carbonyl2-phenethylpropane

Base Information

Chemical Name:2-(Et-thio)carbonyl2-phenethylpropane
CAS No.:112303-76-1
Molecular Formula:C₁₄H₂₀OS
Molecular Weight:236.378
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(Et-thio)carbonyl2-phenethylpropane

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Technology Process of 2-(Et-thio)carbonyl2-phenethylpropane

There total 4 articles about 2-(Et-thio)carbonyl2-phenethylpropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112303-72-7
2-Bromomethyl-2-methyl-4-phenyl-thiobutyric acid S-ethyl ester

: 112303-76-1
2-(Et-thio)carbonyl2-phenethylpropane

Guidance literature:: With tri-n-butyl-tin hydride; In benzene;
DOI:10.1246/cl.1987.409

Reference yield:

: 2-(Et-thio)carbonyl-2-phenethylpropyl cobaloxime

: 112303-76-1
2-(Et-thio)carbonyl2-phenethylpropane

: 112303-80-7
3-Methylene-5-phenyl-pentanethioic acid S-ethyl ester

: 112303-83-0
2-Methyl-1,2,3,4-tetrahydro-naphthalene-2-carbothioic acid S-ethyl ester

Guidance literature:: In chloroform; Irradiation (UV/VIS); irradiation of soln. of Co-compd. by a high pressure mercury lamp (400 W); chromy. on silica gel (CHCl3), sepn. by TLC, total yield 80-90 %, ratio phenethylpropane/tetraline = 75:25;
DOI:10.1246/cl.1987.409