2,12b-dimethyl-1,3-diphenyl-8,12b-dihydrodibenzo-8-thiaazulene

Base Information

Chemical Name:2,12b-dimethyl-1,3-diphenyl-8,12b-dihydrodibenzo-8-thiaazulene
CAS No.:77189-55-0
Molecular Formula:C₃₁H₂₄S
Molecular Weight:428.598
Hs Code.:

2,12b-dimethyl-1,3-diphenyl-8,12b-dihydrodibenzo<e,h>-8-thiaazulene

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,12b-dimethyl-1,3-diphenyl-8,12b-dihydrodibenzo-8-thiaazulene

Chemical Property:

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Technology Process of 2,12b-dimethyl-1,3-diphenyl-8,12b-dihydrodibenzo-8-thiaazulene

There total 6 articles about 2,12b-dimethyl-1,3-diphenyl-8,12b-dihydrodibenzo-8-thiaazulene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 77189-41-4
1,3-Diphenyl-2,8-dihydrodibenzo-8-thiaazulene

: 74-88-4
methyl iodide

: 77189-42-5
1,3-diphenyl-2,8-dihydrodibenzo-8-thiaazulen-2-one

: 77189-50-5
1,3-diphenyl-12b-methyl-8,12b-dihydrodibenzo-8-thiaazulene

: 77189-55-0
2,12b-dimethyl-1,3-diphenyl-8,12b-dihydrodibenzo-8-thiaazulene

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 2.) excess CH₃I,;
DOI:10.1016/S0040-4039(00)92885-5

Reference yield:

: 77189-49-2
1,3-Diphenyl-8-methyldibenzo-8-thiaazulene

: 77189-55-0
2,12b-dimethyl-1,3-diphenyl-8,12b-dihydrodibenzo-8-thiaazulene

Guidance literature:: Multi-step reaction with 3 steps

1: 12 percent / tetrahydrofuran / Heating

2: 1.) NaH,

3: 1.) NaH,

With sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)92885-5

Reference yield:

: 77189-41-4
1,3-Diphenyl-2,8-dihydrodibenzo-8-thiaazulene

: 77189-55-0
2,12b-dimethyl-1,3-diphenyl-8,12b-dihydrodibenzo-8-thiaazulene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH,

2: 1.) NaH,

With sodium hydride;
DOI:10.1016/S0040-4039(00)92885-5