Technology Process of 2(3H)-Furanone, dihydro-5-(4-methoxyphenyl)-, (5S)-
There total 30 articles about 2(3H)-Furanone, dihydro-5-(4-methoxyphenyl)-, (5S)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
tert-butyl 4-(4-methoxyphenyl)-4-oxobutanoate;
With
[RuBr2{(S,S)-2,4-bis-[(3,5-diisopropylphenyl)phosphanyl]pentane}(3-aminomethylisoquinoline)]; potassium tert-butylate; hydrogen;
In
ethanol;
at 25 ℃;
for 2h;
under 6000.6 Torr;
Autoclave;
With
potassium tert-butylate;
In
toluene;
at 25 ℃;
enantioselective reaction;
Inert atmosphere;
DOI:10.1002/anie.201711363
- Guidance literature:
-
ethyl 4-(4-methoxyphenyl)butanoate;
With
ketoreductase-P2-C02; oxygen; NADPH; 9-(2-mesityl)-10-methylacridinium perchlorate;
In
water; acetonitrile;
at 23 ℃;
for 24h;
Irradiation;
Enzymatic reaction;
With
isopropyl alcohol;
In
water; acetonitrile;
enantioselective reaction;
Enzymatic reaction;
DOI:10.1002/anie.201909426
- Guidance literature:
-
C13H15N3O3;
With
formic acid; N-[(1S,2S)-1,2-diphenyl-2-(3-phenylpropylamino)ethyl]-4-methylbenzene sulfonamide ammonium chloride ruthenium; triethylamine;
In
water;
at 60 ℃;
for 24h;
Inert atmosphere;
With
trifluoroacetic acid;
In
dichloromethane; water;
for 4h;
Inert atmosphere;
DOI:10.1021/ol501895k