Sodium; (2S,5R,6R)-6-{2-[(4-ethyl-2,3-dioxo-piperazine-1-carbonyl)-amino]-2-phenyl-acetylamino}-3,3-dimethyl-7-oxo-6-((E)-3-oxo-propenyl)-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

Base Information

Chemical Name:Sodium; (2S,5R,6R)-6-{2-[(4-ethyl-2,3-dioxo-piperazine-1-carbonyl)-amino]-2-phenyl-acetylamino}-3,3-dimethyl-7-oxo-6-((E)-3-oxo-propenyl)-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate
CAS No.:94612-24-5
Molecular Formula:C₂₆H₂₈N₅O₈S*Na
Molecular Weight:593.593
Hs Code.:

Sodium; (2S,5R,6R)-6-{2-[(4-ethyl-2,3-dioxo-piperazine-1-carbonyl)-amino]-2-phenyl-acetylamino}-3,3-dimethyl-7-oxo-6-((E)-3-oxo-propenyl)-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

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Chemical Property of Sodium; (2S,5R,6R)-6-{2-[(4-ethyl-2,3-dioxo-piperazine-1-carbonyl)-amino]-2-phenyl-acetylamino}-3,3-dimethyl-7-oxo-6-((E)-3-oxo-propenyl)-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

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Technology Process of Sodium; (2S,5R,6R)-6-{2-[(4-ethyl-2,3-dioxo-piperazine-1-carbonyl)-amino]-2-phenyl-acetylamino}-3,3-dimethyl-7-oxo-6-((E)-3-oxo-propenyl)-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

There total 3 articles about Sodium; (2S,5R,6R)-6-{2-[(4-ethyl-2,3-dioxo-piperazine-1-carbonyl)-amino]-2-phenyl-acetylamino}-3,3-dimethyl-7-oxo-6-((E)-3-oxo-propenyl)-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94612-40-5
6α-(hydroxymethyl)penicillinate

: 94612-24-5
Sodium; (2S,5R,6R)-6-{2-[(4-ethyl-2,3-dioxo-piperazine-1-carbonyl)-amino]-2-phenyl-acetylamino}-3,3-dimethyl-7-oxo-6-((E)-3-oxo-propenyl)-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: SO₃*pyridine, Et₃N / dimethylsulfoxide / 3 h / 20 °C

2: ethyl acetate / 16 h / 20 °C

3: 1.) H₂; 2.) sodium 2-ethylhexanoate / 1.) 10percent Pd/C / 1.) tetrahydrofuran/H₂O

With pyridine-SO₃ complex; hydrogen; triethylamine; sodium 2-ethylhexanoic acid; palladium on activated charcoal; In dimethyl sulfoxide; ethyl acetate;
DOI:10.1016/S0040-4039(01)81535-5

Reference yield:

: 94612-06-3
6α-formyl penicillin

: 94612-24-5
Sodium; (2S,5R,6R)-6-{2-[(4-ethyl-2,3-dioxo-piperazine-1-carbonyl)-amino]-2-phenyl-acetylamino}-3,3-dimethyl-7-oxo-6-((E)-3-oxo-propenyl)-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: ethyl acetate / 16 h / 20 °C

2: 1.) H₂; 2.) sodium 2-ethylhexanoate / 1.) 10percent Pd/C / 1.) tetrahydrofuran/H₂O

With hydrogen; sodium 2-ethylhexanoic acid; palladium on activated charcoal; In ethyl acetate;
DOI:10.1016/S0040-4039(01)81535-5

Reference yield:

: 94612-17-6
(2S,5R,6R)-6-{2-[(4-Ethyl-2,3-dioxo-piperazine-1-carbonyl)-amino]-2-phenyl-acetylamino}-3,3-dimethyl-7-oxo-6-((E)-3-oxo-propenyl)-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid benzyl ester

: 94612-24-5
Sodium; (2S,5R,6R)-6-{2-[(4-ethyl-2,3-dioxo-piperazine-1-carbonyl)-amino]-2-phenyl-acetylamino}-3,3-dimethyl-7-oxo-6-((E)-3-oxo-propenyl)-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: With hydrogen; sodium 2-ethylhexanoic acid; palladium on activated charcoal; Multistep reaction; 1.) tetrahydrofuran/H₂O;
DOI:10.1016/S0040-4039(01)81535-5