6α-formyl penicillin

Base Information

Chemical Name:6α-formyl penicillin
CAS No.:94612-06-3
Molecular Formula:C₃₁H₃₃N₅O₈S
Molecular Weight:635.698
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6α-formyl penicillin

Chemical Property:

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Technology Process of 6α-formyl penicillin

There total 1 articles about 6α-formyl penicillin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94612-40-5
6α-(hydroxymethyl)penicillinate

: 94612-06-3
6α-formyl penicillin

Guidance literature:: With pyridine-SO₃ complex; triethylamine; In dimethyl sulfoxide; at 20 ℃; for 3h;
DOI:10.1016/S0040-4039(01)81535-5

Reference yield:

: 94612-06-3
6α-formyl penicillin

: 94611-98-0
Sodium; (2S,5R,6R)-6-acetyl-6-{2-[(4-ethyl-2,3-dioxo-piperazine-1-carbonyl)-amino]-2-phenyl-acetylamino}-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 1.5 h / -5 °C

2: 1.) H₂; 2.) sodium 2-ethylhexanoate / 1.) 10 percent Pd/C / 1.) tetrahydrofuran/H₂O

With hydrogen; sodium 2-ethylhexanoic acid; palladium on activated charcoal; In dichloromethane;
DOI:10.1016/S0040-4039(01)81535-5

Reference yield:

: 94612-06-3
6α-formyl penicillin

: 94612-24-5
Sodium; (2S,5R,6R)-6-{2-[(4-ethyl-2,3-dioxo-piperazine-1-carbonyl)-amino]-2-phenyl-acetylamino}-3,3-dimethyl-7-oxo-6-((E)-3-oxo-propenyl)-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: ethyl acetate / 16 h / 20 °C

2: 1.) H₂; 2.) sodium 2-ethylhexanoate / 1.) 10percent Pd/C / 1.) tetrahydrofuran/H₂O

With hydrogen; sodium 2-ethylhexanoic acid; palladium on activated charcoal; In ethyl acetate;
DOI:10.1016/S0040-4039(01)81535-5