p-Methoxybenzyl 7-<(Z)-2-(2-tritylaminothiazol-4-yl)-2-(1-diphenylmethoxycarbonyl-1-methyl)ethoxyiminoacetamido>-3-(3-hydroxy-1-pyridinio)methyl-3-cephem-4-carboxylate Iodide

Base Information

Chemical Name:p-Methoxybenzyl 7-<(Z)-2-(2-tritylaminothiazol-4-yl)-2-(1-diphenylmethoxycarbonyl-1-methyl)ethoxyiminoacetamido>-3-(3-hydroxy-1-pyridinio)methyl-3-cephem-4-carboxylate Iodide
CAS No.:131580-97-7
Molecular Formula:C₆₂H₅₅N₆O₉S₂*I
Molecular Weight:1219.19
Hs Code.:

p-Methoxybenzyl 7-<(Z)-2-(2-tritylaminothiazol-4-yl)-2-(1-diphenylmethoxycarbonyl-1-methyl)ethoxyiminoacetamido>-3-(3-hydroxy-1-pyridinio)methyl-3-cephem-4-carboxylate Iodide

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Chemical Property of p-Methoxybenzyl 7-<(Z)-2-(2-tritylaminothiazol-4-yl)-2-(1-diphenylmethoxycarbonyl-1-methyl)ethoxyiminoacetamido>-3-(3-hydroxy-1-pyridinio)methyl-3-cephem-4-carboxylate Iodide

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Technology Process of p-Methoxybenzyl 7-<(Z)-2-(2-tritylaminothiazol-4-yl)-2-(1-diphenylmethoxycarbonyl-1-methyl)ethoxyiminoacetamido>-3-(3-hydroxy-1-pyridinio)methyl-3-cephem-4-carboxylate Iodide

There total 3 articles about p-Methoxybenzyl 7-<(Z)-2-(2-tritylaminothiazol-4-yl)-2-(1-diphenylmethoxycarbonyl-1-methyl)ethoxyiminoacetamido>-3-(3-hydroxy-1-pyridinio)methyl-3-cephem-4-carboxylate Iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 127800-40-2
p-Methoxybenzyl 7-<(Z)-2-(2-tritylaminothiazol-4-yl)-2-(1-diphenylmethoxycarbonyl-1-methyl)ethoxyiminoacetamido>-3-chloromethyl-3-cephem-4-carboxylate

: 131580-97-7
p-Methoxybenzyl 7-<(Z)-2-(2-tritylaminothiazol-4-yl)-2-(1-diphenylmethoxycarbonyl-1-methyl)ethoxyiminoacetamido>-3-(3-hydroxy-1-pyridinio)methyl-3-cephem-4-carboxylate Iodide

Guidance literature:: Multi-step reaction with 2 steps

1: NaI / acetone / 1 h

2: ethyl acetate / 3 h / Ambient temperature

With sodium iodide; In ethyl acetate; acetone;
DOI:10.1248/cpb.38.2271

Reference yield:

: 109-00-2
3-HYDROXYPYRIDINE

: 131580-97-7
p-Methoxybenzyl 7-<(Z)-2-(2-tritylaminothiazol-4-yl)-2-(1-diphenylmethoxycarbonyl-1-methyl)ethoxyiminoacetamido>-3-(3-hydroxy-1-pyridinio)methyl-3-cephem-4-carboxylate Iodide

Guidance literature:: Multi-step reaction with 2 steps

1: ethyl acetate / Ambient temperature

2: ethyl acetate / 3 h / Ambient temperature

In ethyl acetate;
DOI:10.1248/cpb.38.2271