[PdI₂(N,N,N′,N′-tetramethylethylenediamine)]

Base Information

Chemical Name:[PdI₂(N,N,N′,N′-tetramethylethylenediamine)]
CAS No.:86272-80-2
Molecular Formula:C₆H₁₆I₂N₂Pd
Molecular Weight:476.435
Hs Code.:

[PdI<sub>2</sub>(N,N,N′,N′-tetramethylethylenediamine)]

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [PdI₂(N,N,N′,N′-tetramethylethylenediamine)]

Chemical Property:

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Technology Process of [PdI₂(N,N,N′,N′-tetramethylethylenediamine)]

There total 4 articles about [PdI₂(N,N,N′,N′-tetramethylethylenediamine)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 773887-40-4
[palladium(2-(OH)C₆H₄)I(N,N,N',N'-tetramethylethylenediamine)]

: 201230-82-2
carbon monoxide

: 86272-80-2
[PdI₂(N,N,N′,N′-tetramethylethylenediamine)]

: 773887-48-2
[[Pd(C(O)C₆H₄OH-2)I(N,N,N',N'-tetramethylethylenediamine)]

Guidance literature:: In dichloromethane; CO was bubbled through soln. of Pd complex in CH2Cl2 for 30 min; soln. was stirred for 3 h under CO; concd.; Et2O added; filtered; washed (Et2O); dried; elem. anal.;
DOI:10.1021/om0496131

Reference yield: 60.0%

: 868158-56-9
[Pd(C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(N,N,N',N'-tetramethylethylenediamine)]

: 201230-82-2
carbon monoxide

: 86272-80-2
[PdI₂(N,N,N′,N′-tetramethylethylenediamine)]

: 868158-48-9
[Pd(C(O)C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(N,N,N',N'-tetramethylethylenediamine)]

Guidance literature:: In tetrahydrofuran; byproducts: Pd; bubbling CO through a soln. of palladium complex in THF for 10 min, stirring for 20 h under CO atm.; filtration through anhyd. MgSO4, concn., addn. of n-pentane, stirring, filtration, washing ppt. with n-pentane, drying in air, recrystn. (acetone/Et2O); elem. anal.;
DOI:10.1021/om050451y

Reference yield: 32.0%

: Pd2(dba)4

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: 710316-98-6
1-(2-iodophenyl)-3-p-tolylurea

: 86272-80-2
[PdI₂(N,N,N′,N′-tetramethylethylenediamine)]

: 868158-56-9
[Pd(C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(N,N,N',N'-tetramethylethylenediamine)]

Guidance literature:: In toluene; (N2); stirring a mixt. of palladium complex with ligand in toluene for 10 min, addn. of urea deriv., stirring for 4 h; evapn., addn. of CH2Cl2, filtration through anhyd. MgSO4, evapn., addn. of Et2O, filtration, washing with Et2O, drying in air, layering Et2O over a concd. soln. in CH2Cl2, standing overnight, filtration, air drying; elem. anal.;
DOI:10.1021/om050451y