(C₅H₅)Fe(C₅H₄CONHCH(CH₂C₆H₅)COOCH₃)

Base Information

Chemical Name:(C₅H₅)Fe(C₅H₄CONHCH(CH₂C₆H₅)COOCH₃)
CAS No.:181589-81-1
Molecular Formula:C₂₁H₂₁FeNO₃
Molecular Weight:391.25
Hs Code.:

(C<sub>5</sub>H<sub>5</sub>)Fe(C<sub>5</sub>H<sub>4</sub>CONHCH(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)COOCH<sub>3</sub>)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (C₅H₅)Fe(C₅H₄CONHCH(CH₂C₆H₅)COOCH₃)

Chemical Property:

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Technology Process of (C₅H₅)Fe(C₅H₄CONHCH(CH₂C₆H₅)COOCH₃)

There total 1 articles about (C₅H₅)Fe(C₅H₄CONHCH(CH₂C₆H₅)COOCH₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1271-42-7
ferrocenecarboxylic acid

: 5619-07-8
methyl 2-amino-3-phenylpropanoate hydrochloride

: 181589-81-1,1093682-66-6
(C₅H₅)Fe(C₅H₄CONHCH(CH₂C₆H₅)COOCH₃)

Guidance literature:: With dicyclohexylcarbodiimide; HOBt; Et₃N; In dichloromethane; byproducts: dicyclohexylurea; N2-atmosphere; treatment of Fe-complex with excess of dicyclohexylcarbodiimide and HOBt, treatment of amino acid ester with equimolar amt. of NEt3, addn. to Fe-complex soln., stirring for 14-20 h; filtration off of urea derivative, washing (H2O), drying (MgSO4), solvent removal (vac.), recrystn. (EtOAc);
DOI:10.1016/S0022-328X(99)00009-1

Reference yield:

: 181589-81-1,1093682-66-6
(C₅H₅)Fe(C₅H₄CONHCH(CH₂C₆H₅)COOCH₃)

: (C₅H₅)Fe(C₅H₄CONHCH(CH₂C₆H₅)COOH)

Guidance literature:: With NaOH; HCl; In not given; N2-atmosphere; addn. of slight excess of 0.1 N NaOH to Fe-complex soln. (in EtOH or EtOH/THF, not specified) at 0°C, stirring for 2-4 h, distn. off of solvents, cooling to 0°C, dropwise addn. of 0.1 N HCl (pptn.); filtration, washing (H2O), drying (vac., several h);
DOI:10.1016/S0022-328X(99)00009-1