Technology Process of C10H8F4O
There total 1 articles about C10H8F4O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
(S)-5-benzyl-2,2,3,-trimethylimidazolidin-4-one dichloroacetic acid salt; N-fluorobis(benzenesulfon)imide;
In
tetrahydrofuran; isopropyl alcohol;
at -15 ℃;
DOI:10.1039/c2ob26402a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium aluminium tetrahydride / 17 h / -15 °C
2: triethylamine; dmap / dichloromethane / 18 h / 0 - 20 °C
3: toluene / 16 h / Reflux
4: hydrogenchloride / diethyl ether
With
hydrogenchloride; dmap; lithium aluminium tetrahydride; triethylamine;
In
diethyl ether; dichloromethane; toluene;
DOI:10.1039/c2ob26402a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium aluminium tetrahydride / 17 h / -15 °C
2: triethylamine; dmap / dichloromethane / 18 h / 0 - 20 °C
3: toluene / 16 h / Reflux
With
dmap; lithium aluminium tetrahydride; triethylamine;
In
dichloromethane; toluene;
DOI:10.1039/c2ob26402a