benzyl 4-O-amino-2,3-O-isopropylidene-α-D-arabinoside

Base Information

Chemical Name:benzyl 4-O-amino-2,3-O-isopropylidene-α-D-arabinoside
CAS No.:478175-70-1
Molecular Formula:C₁₅H₂₁NO₅
Molecular Weight:295.335
Hs Code.:

Synonyms:

Suppliers and Price of benzyl 4-O-amino-2,3-O-isopropylidene-α-D-arabinoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl 4-O-amino-2,3-O-isopropylidene-α-D-arabinoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl 4-O-amino-2,3-O-isopropylidene-α-D-arabinoside

There total 6 articles about benzyl 4-O-amino-2,3-O-isopropylidene-α-D-arabinoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 478175-68-7
benzyl 2,3-O-isopropylidene-4-O-(N-phthalimido)-α-D-arabinoside

: 478175-70-1
benzyl 4-O-amino-2,3-O-isopropylidene-α-D-arabinoside

Guidance literature:: With hydrazine hydrate; In chloroform;
DOI:10.1139/v02-060

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 478175-70-1
benzyl 4-O-amino-2,3-O-isopropylidene-α-D-arabinoside

Guidance literature:: Multi-step reaction with 5 steps

1.1: BF₃*OEt₂; molecular sieves 3 Angstroem / CH₂Cl₂ / 4 h

1.2: acetic anhydride; pyridine / CH₂Cl₂ / 2 h

2.1: 26.2 g / sodium / methanol / 3 h

3.1: 60 percent / hydrogen chloride / methanol; dimethylformamide / 1 h / 20 °C

4.1: 68 percent / triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 72 h / 20 °C

5.1: 1.2 g / hydrazine hydrate / CHCl₃

With hydrogenchloride; di-isopropyl azodicarboxylate; 3 A molecular sieve; boron trifluoride diethyl etherate; sodium; hydrazine hydrate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; chloroform; N,N-dimethyl-formamide; 4.1: Mitsunobu reaction;
DOI:10.1139/v02-060

Reference yield:

: 478175-99-4
benzyl β-L-xylopyranoside

: 478175-70-1
benzyl 4-O-amino-2,3-O-isopropylidene-α-D-arabinoside

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / hydrogen chloride / methanol; dimethylformamide / 1 h / 20 °C

2: 68 percent / triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 72 h / 20 °C

3: 1.2 g / hydrazine hydrate / CHCl₃

With hydrogenchloride; di-isopropyl azodicarboxylate; hydrazine hydrate; triphenylphosphine; In tetrahydrofuran; methanol; chloroform; N,N-dimethyl-formamide; 2: Mitsunobu reaction;
DOI:10.1139/v02-060