[Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)]OSO₂CF₃

Base Information

Chemical Name:[Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)]OSO₂CF₃
CAS No.:334912-11-7
Molecular Formula:CF₃O₃S*C₃₄H₃₃N₂O₃PdS₂
Molecular Weight:837.27
Hs Code.:

[Pd<sub>2</sub>(k2-C,S-CH(STol-p)(C<sub>6</sub>H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)]OSO<sub>2</sub>CF<sub>3</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)]OSO₂CF₃

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Technology Process of [Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)]OSO₂CF₃

There total 3 articles about [Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)]OSO₂CF₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 366-18-7
[2,2]bipyridinyl

: 334912-05-9
[Pd2(k2-C,S-CH(STol-p)(C6H(STol-p-2)(OMe)3-3,4,5))2(μ-I)2]

: 73491-36-8
thallium(I) triflate

: 334912-11-7
[Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)]OSO₂CF₃

Guidance literature:: In dichloromethane; Tl-salt and complex were stirred in CH2Cl2 for 15 min, 2,2'-bipyridine was added, the mixt. was stirred for 8 h; filtered, concd., Et2O was added, ppt. was filtered, washed with Et2O, dried in an oven at 70°C for 2 h, and over P2O5 for 2 days; elem. anal.;
DOI:10.1021/om0008981

Reference yield: 85.0%

: 334912-04-8
[Pd(k2-C,S-C₆H(OMe)3-2,3,4-CH(STol-p)2-6)(2,2'-bipyridine)]O₃SCF₃

: 334912-11-7
[Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)]OSO₂CF₃

Guidance literature:: In 1,2-dichloro-ethane; a soln. in 1,2-dichloroethane was reafluxed for 8 h; concd., Et2O was added;
DOI:10.1021/om0008981

Reference yield:

: 366-18-7
[2,2]bipyridinyl

: 334912-11-7
[Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)]OSO₂CF₃

Guidance literature:: Multi-step reaction with 2 steps

1: toluene

2: 1,2-dichloro-ethane

In 1,2-dichloro-ethane; toluene;
DOI:10.1021/om0008981