CpCr[(XylNCMe)2CH](CH₂CMe₃)

Base Information

Chemical Name:CpCr[(XylNCMe)2CH](CH₂CMe₃)
CAS No.:1203470-67-0
Molecular Formula:C₃₁H₄₁CrN₂
Molecular Weight:493.676
Hs Code.:

CpCr[(XylNCMe)2CH](CH<sub>2</sub>CMe<sub>3</sub>)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of CpCr[(XylNCMe)2CH](CH₂CMe₃)

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Technology Process of CpCr[(XylNCMe)2CH](CH₂CMe₃)

There total 1 articles about CpCr[(XylNCMe)2CH](CH₂CMe₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: Mg(neopentyl)2*1.05(1,4-dioxane)

: 1203470-66-9
[Cr(cyclopentadienyl)((xylyl)NC(Me)CHC(Me)N(xylyl))(tosylato)]

: 1203470-67-0
CpCr[(XylNCMe)2CH](CH₂CMe₃)

Guidance literature:: In diethyl ether; (N2); using Schlenk techniques; addn. of Et2O to CrCp((xylyl)NHCMeCHCMeN(xylyl))(OTs); addn. dropwise of soln. of Mg(CH2CMe3)2*1.05(1,4-dioxane); stirring for 1.5 h at room temp.; evapn. of solvent in vac., extn. with hexanes; filtration; rinsing with hexanes; evapn. of solvent in vac., extn. with hexanes; filtration, cooling to -35°C; crystn. over several ds, elem. anal.;
DOI:10.1021/om900869p

Reference yield: 23.0%

: 108-05-4,9003-20-7
vinyl acetate

: 1203470-67-0
CpCr[(XylNCMe)2CH](CH₂CMe₃)

: 1203470-68-1
[Cr(cyclopentadienyl)((xylyl)NC(Me)CHC(Me)N(xylyl))(OC(O)Me)]

Guidance literature:: In further solvent(s); (N2); using Schlenk techniques; evacuating of thermolyzed mixt. of CrCp((xylyl)NHCMeCHCMeN(xylyl))(neopentyl) in vinyl acetate; extn. with Et2O; filtration, concn., cooling to -35°C for 2 weeks; crystn.;
DOI:10.1021/om900869p