[Cr(cyclopentadienyl)((xylyl)NC(Me)CHC(Me)N(xylyl))(tosylato)]

Base Information

Chemical Name:[Cr(cyclopentadienyl)((xylyl)NC(Me)CHC(Me)N(xylyl))(tosylato)]
CAS No.:1203470-66-9
Molecular Formula:C₃₃H₃₇CrN₂O₃S
Molecular Weight:593.73
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Cr(cyclopentadienyl)((xylyl)NC(Me)CHC(Me)N(xylyl))(tosylato)]

Chemical Property:

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Technology Process of [Cr(cyclopentadienyl)((xylyl)NC(Me)CHC(Me)N(xylyl))(tosylato)]

There total 2 articles about [Cr(cyclopentadienyl)((xylyl)NC(Me)CHC(Me)N(xylyl))(tosylato)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1198298-27-9
[Cr(cyclopentadienyl)((xylyl)NC(Me)CHC(Me)N(xylyl))Cl]

: 16836-95-6
silver(I) 4-methylbenzenesulfonate

: 1203470-66-9
[Cr(cyclopentadienyl)((xylyl)NC(Me)CHC(Me)N(xylyl))(tosylato)]

Guidance literature:: In tetrahydrofuran; (N2); using Schlenk techniques; addn. of THF to mixt. of CrCp((xylyl)NHCMeCHCMeN(xylyl))Cl and AgOTs; stirring overnight at room temp.; filtration, evapn. of solvent in vac., extn. with hexanes/CH2Cl2 mixt. (4:1); filtration; rinsing with hexanes; cooling to -20°C; crystn.over several days, elem. anal.;
DOI:10.1021/om900869p

Reference yield:

: 59229-09-3
2,4,6-collidinium p-toluenesulfonate

: (CpCr[(2,6-Me2C6H3NCMe)2CH])2(μ-O)

: 1203470-66-9
[Cr(cyclopentadienyl)((xylyl)NC(Me)CHC(Me)N(xylyl))(tosylato)]

: 1351668-55-7
CpCr[(2,6-Me₂C₆H₃NCMe)2CH](OH)

Guidance literature:: In not given;
DOI:10.1021/ic202233f

Reference yield: 69.0%

: 1203470-66-9
[Cr(cyclopentadienyl)((xylyl)NC(Me)CHC(Me)N(xylyl))(tosylato)]

: 563-63-3
silver(I) acetate

: 1203470-68-1
[Cr(cyclopentadienyl)((xylyl)NC(Me)CHC(Me)N(xylyl))(OC(O)Me)]

Guidance literature:: In tetrahydrofuran; (N2); using Schlenk techniques; addn. of THF to mixt. of CrCp((xylyl)NHCMeCHCMeN(xylyl))Cl and AgOAc; stirring overnight at room temp. in the absence of light; evapn. of solvent in vac., extn. with hexanes/CH2Cl2 mixt. (3:1); filtration; rinsing with hexanes; cooling to-20°C; crystn. over severalds;
DOI:10.1021/om900869p