Benzoic acid, 4-(decyloxy)-, 4-(phenylmethoxy)phenyl ester

Base Information

• Chemical Name: Benzoic acid, 4-(decyloxy)-, 4-(phenylmethoxy)phenyl ester
• CAS No.: 129561-09-7
• Molecular Formula: C30H36O4
• Molecular Weight: 460.613
• Mol file: 129561-09-7.mol

Synonyms:

Chemical Property of Benzoic acid, 4-(decyloxy)-, 4-(phenylmethoxy)phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 4-(decyloxy)-, 4-(phenylmethoxy)phenyl ester

There total 2 articles about Benzoic acid, 4-(decyloxy)-, 4-(phenylmethoxy)phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Benzyloxyphenol (103-16-2) + 4-decyloxybenzoyl chloride (50625-44-0) → 4-Decyloxy-benzoic acid 4-benzyloxy-phenyl ester (129561-09-7)

Guidance literature:

With triethylamine; In dichloromethane; for 2h; Yield given; Heating;

DOI:10.1002/hlca.19930760210

Reference yield:

p-decyloxybenzoic acid (5519-23-3) → 4-Decyloxy-benzoic acid 4-benzyloxy-phenyl ester (129561-09-7)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂ / 2 h / Heating

2: NEt₃ / CH₂Cl₂ / 2 h / Heating

With thionyl chloride; triethylamine; In dichloromethane;

DOI:10.1002/hlca.19930760210

Reference yield:

4-Decyloxy-benzoic acid 4-benzyloxy-phenyl ester (129561-09-7) → 4-hydroxyphenyl 4'-n-decyloxybenzoate (124249-85-0)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; dichloromethane; under 15001.2 Torr; Yield given;

DOI:10.1002/hlca.19930760210

upstream raw materials:

4-Benzyloxyphenol

4-decyloxybenzoyl chloride

p-decyloxybenzoic acid

Downstream raw materials:

4-hydroxyphenyl 4'-n-decyloxybenzoate

C₃₇H₄₀O₆

4-{[(4-decyloxyphenyl)carbonyl]oxy}phenyl thiophene-2-carboxylate

4-{[(4-decyloxyphenyl)carbonyl]oxy}phenyl thiophene-3-carboxylate

Refernces

• 1、 Sakurai, Y.,Tamatani, A.,Teshima, K.,Kusabayashi, S.,Takenaka, S.. "Molecular Structure and Liquid Crystalline Properties: The Effect of the Terminal Hydroxy Group on Mesomorphic Properties". . p. 163 - 172. Retrieved 2007/10/02.