2-Naphthalenecarboxylic acid, 1-bromo-, phenyl ester

Base Information

Chemical Name:2-Naphthalenecarboxylic acid, 1-bromo-, phenyl ester
CAS No.:129667-82-9
Molecular Formula:C17H11BrO2
Molecular Weight:327.177
Hs Code.:

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Chemical Property of 2-Naphthalenecarboxylic acid, 1-bromo-, phenyl ester

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Technology Process of 2-Naphthalenecarboxylic acid, 1-bromo-, phenyl ester

There total 3 articles about 2-Naphthalenecarboxylic acid, 1-bromo-, phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 76373-11-0
1-bromo-2-naphthoyl chloride

: 108-95-2,27073-41-2
phenol

: 129667-82-9
phenyl 1-bromo-2-naphthoate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1039/c5cc01074h

Reference yield: 37.0%

: 20717-79-7
1-bromo-2-naphthoic acid

: 108-95-2,27073-41-2
phenol

: 129667-82-9
phenyl 1-bromo-2-naphthoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1021/jacs.9b13117

Reference yield:

: 20717-79-7
1-bromo-2-naphthoic acid

: 129667-82-9
phenyl 1-bromo-2-naphthoate

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / dichloromethane / 1 h / 0 - 20 °C

2: pyridine / dichloromethane / 18 h / 20 °C

With pyridine; oxalyl dichloride; In dichloromethane;
DOI:10.1039/c5cc01074h