(3S,6S,9S,12R,15S,18S)-3,9-Bis-(4-amino-butyl)-18-benzyl-15-(4-hydroxy-benzyl)-12-(1H-indol-3-ylmethyl)-6-isopropyl-1-methyl-1,4,7,10,13,16-hexaaza-cyclooctadecane-2,5,8,11,14,17-hexaone

Base Information

Chemical Name:(3S,6S,9S,12R,15S,18S)-3,9-Bis-(4-amino-butyl)-18-benzyl-15-(4-hydroxy-benzyl)-12-(1H-indol-3-ylmethyl)-6-isopropyl-1-methyl-1,4,7,10,13,16-hexaaza-cyclooctadecane-2,5,8,11,14,17-hexaone
CAS No.:137506-31-1
Molecular Formula:C₄₇H₆₃N₉O₇
Molecular Weight:866.073
Hs Code.:

(3S,6S,9S,12R,15S,18S)-3,9-Bis-(4-amino-butyl)-18-benzyl-15-(4-hydroxy-benzyl)-12-(1H-indol-3-ylmethyl)-6-isopropyl-1-methyl-1,4,7,10,13,16-hexaaza-cyclooctadecane-2,5,8,11,14,17-hexaone

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Chemical Property of (3S,6S,9S,12R,15S,18S)-3,9-Bis-(4-amino-butyl)-18-benzyl-15-(4-hydroxy-benzyl)-12-(1H-indol-3-ylmethyl)-6-isopropyl-1-methyl-1,4,7,10,13,16-hexaaza-cyclooctadecane-2,5,8,11,14,17-hexaone

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Technology Process of (3S,6S,9S,12R,15S,18S)-3,9-Bis-(4-amino-butyl)-18-benzyl-15-(4-hydroxy-benzyl)-12-(1H-indol-3-ylmethyl)-6-isopropyl-1-methyl-1,4,7,10,13,16-hexaaza-cyclooctadecane-2,5,8,11,14,17-hexaone

There total 3 articles about (3S,6S,9S,12R,15S,18S)-3,9-Bis-(4-amino-butyl)-18-benzyl-15-(4-hydroxy-benzyl)-12-(1H-indol-3-ylmethyl)-6-isopropyl-1-methyl-1,4,7,10,13,16-hexaaza-cyclooctadecane-2,5,8,11,14,17-hexaone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 137506-37-7
C₆₉H₇₈N₁₀O₁₁

: 137506-31-1
(3S,6S,9S,12R,15S,18S)-3,9-Bis-(4-amino-butyl)-18-benzyl-15-(4-hydroxy-benzyl)-12-(1H-indol-3-ylmethyl)-6-isopropyl-1-methyl-1,4,7,10,13,16-hexaaza-cyclooctadecane-2,5,8,11,14,17-hexaone

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / CH₂Cl₂

With piperidine; In dichloromethane;
DOI:10.1016/S0040-4039(00)92279-2

Reference yield:

: 137506-35-5
C₆₉H₈₀N₁₀O₁₂

: 137506-31-1
(3S,6S,9S,12R,15S,18S)-3,9-Bis-(4-amino-butyl)-18-benzyl-15-(4-hydroxy-benzyl)-12-(1H-indol-3-ylmethyl)-6-isopropyl-1-methyl-1,4,7,10,13,16-hexaaza-cyclooctadecane-2,5,8,11,14,17-hexaone

Guidance literature:: Multi-step reaction with 3 steps

1: DPPA, NaHCO₃ / dimethylformamide

2: piperidine / CH₂Cl₂

With piperidine; diphenyl-phosphinic acid; sodium hydrogencarbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)92279-2