{4-[(2S,5S,8S,11R,14S,17S)-14-(4-Amino-butyl)-5-benzyl-8-(4-hydroxy-benzyl)-11-(1H-indol-3-ylmethyl)-17-isopropyl-4-methyl-3,6,9,12,15,18-hexaoxo-1,4,7,10,13,16-hexaaza-cyclooctadec-2-yl]-butyl}-carbamic acid pyridin-4-ylmethyl ester

Base Information

Chemical Name:{4-[(2S,5S,8S,11R,14S,17S)-14-(4-Amino-butyl)-5-benzyl-8-(4-hydroxy-benzyl)-11-(1H-indol-3-ylmethyl)-17-isopropyl-4-methyl-3,6,9,12,15,18-hexaoxo-1,4,7,10,13,16-hexaaza-cyclooctadec-2-yl]-butyl}-carbamic acid pyridin-4-ylmethyl ester
CAS No.:137506-41-3
Molecular Formula:C₅₄H₆₈N₁₀O₉
Molecular Weight:1001.2
Hs Code.:

{4-[(2S,5S,8S,11R,14S,17S)-14-(4-Amino-butyl)-5-benzyl-8-(4-hydroxy-benzyl)-11-(1H-indol-3-ylmethyl)-17-isopropyl-4-methyl-3,6,9,12,15,18-hexaoxo-1,4,7,10,13,16-hexaaza-cyclooctadec-2-yl]-butyl}-carbamic acid pyridin-4-ylmethyl ester

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Chemical Property of {4-[(2S,5S,8S,11R,14S,17S)-14-(4-Amino-butyl)-5-benzyl-8-(4-hydroxy-benzyl)-11-(1H-indol-3-ylmethyl)-17-isopropyl-4-methyl-3,6,9,12,15,18-hexaoxo-1,4,7,10,13,16-hexaaza-cyclooctadec-2-yl]-butyl}-carbamic acid pyridin-4-ylmethyl ester

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Technology Process of {4-[(2S,5S,8S,11R,14S,17S)-14-(4-Amino-butyl)-5-benzyl-8-(4-hydroxy-benzyl)-11-(1H-indol-3-ylmethyl)-17-isopropyl-4-methyl-3,6,9,12,15,18-hexaoxo-1,4,7,10,13,16-hexaaza-cyclooctadec-2-yl]-butyl}-carbamic acid pyridin-4-ylmethyl ester

There total 2 articles about {4-[(2S,5S,8S,11R,14S,17S)-14-(4-Amino-butyl)-5-benzyl-8-(4-hydroxy-benzyl)-11-(1H-indol-3-ylmethyl)-17-isopropyl-4-methyl-3,6,9,12,15,18-hexaoxo-1,4,7,10,13,16-hexaaza-cyclooctadec-2-yl]-butyl}-carbamic acid pyridin-4-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 137506-37-7
C₆₉H₇₈N₁₀O₁₁

: 137506-41-3
{4-[(2S,5S,8S,11R,14S,17S)-14-(4-Amino-butyl)-5-benzyl-8-(4-hydroxy-benzyl)-11-(1H-indol-3-ylmethyl)-17-isopropyl-4-methyl-3,6,9,12,15,18-hexaoxo-1,4,7,10,13,16-hexaaza-cyclooctadec-2-yl]-butyl}-carbamic acid pyridin-4-ylmethyl ester

Guidance literature:: With piperidine; In dichloromethane;
DOI:10.1016/S0040-4039(00)92279-2

Reference yield:

: 137506-35-5
C₆₉H₈₀N₁₀O₁₂

: 137506-41-3
{4-[(2S,5S,8S,11R,14S,17S)-14-(4-Amino-butyl)-5-benzyl-8-(4-hydroxy-benzyl)-11-(1H-indol-3-ylmethyl)-17-isopropyl-4-methyl-3,6,9,12,15,18-hexaoxo-1,4,7,10,13,16-hexaaza-cyclooctadec-2-yl]-butyl}-carbamic acid pyridin-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: DPPA, NaHCO₃ / dimethylformamide

2: piperidine / CH₂Cl₂

With piperidine; diphenyl-phosphinic acid; sodium hydrogencarbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)92279-2