(5S,8R,9S,10S,13R,14S,17R)-3-[1-Chloro-1-(toluene-4-sulfinyl)-ethyl]-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-ol

Base Information

Chemical Name:(5S,8R,9S,10S,13R,14S,17R)-3-[1-Chloro-1-(toluene-4-sulfinyl)-ethyl]-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-ol
CAS No.:134970-39-1
Molecular Formula:C₃₆H₅₇ClO₂S
Molecular Weight:589.366
Hs Code.:

(5S,8R,9S,10S,13R,14S,17R)-3-[1-Chloro-1-(toluene-4-sulfinyl)-ethyl]-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-ol

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Chemical Property of (5S,8R,9S,10S,13R,14S,17R)-3-[1-Chloro-1-(toluene-4-sulfinyl)-ethyl]-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-ol

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Technology Process of (5S,8R,9S,10S,13R,14S,17R)-3-[1-Chloro-1-(toluene-4-sulfinyl)-ethyl]-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-ol

There total 1 articles about (5S,8R,9S,10S,13R,14S,17R)-3-[1-Chloro-1-(toluene-4-sulfinyl)-ethyl]-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50635-71-7,50635-72-8,31350-93-3
1-chloroethyl p-tolyl sulfoxide

: 566-88-1
dihydrocholesterone

: 134970-39-1
(5S,8R,9S,10S,13R,14S,17R)-3-[1-Chloro-1-(toluene-4-sulfinyl)-ethyl]-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-ol

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1) THF, -60 deg C, 10 min;
DOI:10.1021/jo00013a011

Reference yield:

: 134970-39-1
(5S,8R,9S,10S,13R,14S,17R)-3-[1-Chloro-1-(toluene-4-sulfinyl)-ethyl]-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-ol

: 134970-60-8
(3R,5S,8R,9S,10S,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthrene-3-carboxylic acid benzylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / xylene / Heating

2: 1) ozone, 2) Me₂S / 1) CH₂Cl₂, -60 deg C, 2) to room temperature

With dimethylsulfide; ozone; In xylene;
DOI:10.1021/jo00013a011