(3R,5S,8R,9S,10S,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthrene-3-carboxylic acid benzylamide

Base Information

Chemical Name:(3R,5S,8R,9S,10S,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthrene-3-carboxylic acid benzylamide
CAS No.:134970-60-8
Molecular Formula:C₃₅H₅₅NO₂
Molecular Weight:521.827
Hs Code.:

(3R,5S,8R,9S,10S,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthrene-3-carboxylic acid benzylamide

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Chemical Property of (3R,5S,8R,9S,10S,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthrene-3-carboxylic acid benzylamide

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Technology Process of (3R,5S,8R,9S,10S,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthrene-3-carboxylic acid benzylamide

There total 3 articles about (3R,5S,8R,9S,10S,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthrene-3-carboxylic acid benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 566-88-1
dihydrocholesterone

: 134970-60-8
(3R,5S,8R,9S,10S,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthrene-3-carboxylic acid benzylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1) LDA / 1) THF, -60 deg C, 10 min

2: 97 percent / xylene / Heating

3: 1) ozone, 2) Me₂S / 1) CH₂Cl₂, -60 deg C, 2) to room temperature

With dimethylsulfide; ozone; lithium diisopropyl amide; In xylene;
DOI:10.1021/jo00013a011

Reference yield:

: 134970-39-1
(5S,8R,9S,10S,13R,14S,17R)-3-[1-Chloro-1-(toluene-4-sulfinyl)-ethyl]-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-ol

: 134970-60-8
(3R,5S,8R,9S,10S,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthrene-3-carboxylic acid benzylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / xylene / Heating

2: 1) ozone, 2) Me₂S / 1) CH₂Cl₂, -60 deg C, 2) to room temperature

With dimethylsulfide; ozone; In xylene;
DOI:10.1021/jo00013a011

Reference yield:

: 134970-44-8
(3R,5S,8R,9S,10S,13R,14S,17R)-3-(1-Chloro-vinyl)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-ol

: 100-46-9
benzylamine

: 134970-60-8
(3R,5S,8R,9S,10S,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthrene-3-carboxylic acid benzylamide

Guidance literature:: With dimethylsulfide; ozone; Yield given. Multistep reaction; 1) CH₂Cl₂, -60 deg C, 2) to room temperature;
DOI:10.1021/jo00013a011