Technology Process of C29H28Cl2N2O5
There total 4 articles about C29H28Cl2N2O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hypochlorite / tetrahydrofuran / 20 °C
2: lithium hydroxide; water / tetrahydrofuran; methanol
3: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide
With
4-methyl-morpholine; sodium hypochlorite; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.12.043
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydroxylamine hydrochloride; sodium acetate / ethanol / 20 °C
2: sodium hypochlorite / tetrahydrofuran / 20 °C
3: lithium hydroxide; water / tetrahydrofuran; methanol
4: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide
With
4-methyl-morpholine; sodium hypochlorite; hydroxylamine hydrochloride; water; sodium acetate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide;
In
tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.12.043
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium hydroxide; water / tetrahydrofuran; methanol
2: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide
With
4-methyl-morpholine; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.12.043