potassium tricarbonyl triphenylphosphine cobalt

Base Information

• Chemical Name: potassium tricarbonyl triphenylphosphine cobalt
• CAS No.: 67486-01-5
• Molecular Formula: C₂₁H₁₅CoO₃P*K
• Molecular Weight: 444.414

Synonyms:

Chemical Property of potassium tricarbonyl triphenylphosphine cobalt

Chemical Property:

Purity/Quality:

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Technology Process of potassium tricarbonyl triphenylphosphine cobalt

There total 3 articles about potassium tricarbonyl triphenylphosphine cobalt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

potassium tetracarbonylcobaltate (14878-26-3) → potassium tricarbonyl triphenylphosphine cobalt (67486-01-5)

Guidance literature:

With triphenyl phosphine; In tetrahydrofuran; N2 atmosphere; refluxing (45 min);

Reference yield:

Co(CO)3(CF3CO)(P(C6H5)3) + Dipotassium benzophenone dianion (4460-50-8) → potassium tetracarbonylcobaltate (14878-26-3) + potassium tricarbonyl triphenylphosphine cobalt (67486-01-5)

Guidance literature:

In tetrahydrofuran; acetonitrile; soln. of Co-complex in MeCN reduced by K-salt in THF; monitored by IR;

DOI:10.1016/j.jorganchem.2006.12.027

Reference yield:

Co(CO)3(CF3CO)(P(C6H5)3) + benzophenone radical anion potassium salt (763025-01-0) → potassium tetracarbonylcobaltate (14878-26-3) + potassium tricarbonyl triphenylphosphine cobalt (67486-01-5)

Guidance literature:

In tetrahydrofuran; acetonitrile; soln. of Co-complex in MeCN reduced by K-salt in THF; monitored by IR;

DOI:10.1016/j.jorganchem.2006.12.027

upstream raw materials:

potassium tetracarbonylcobaltate

Dipotassium benzophenone dianion

benzophenone radical anion potassium salt

Downstream raw materials:

{Re(CO)4(P(C₆H₅)3)2}⁽¹⁺⁾*{Co(CO)4}^(1-)={Re(CO)4(P(C₆H₅)3)2}{Co(CO)4}

BiCl(Co(CO)3P(C₆H₅)3)2

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