meso-tetra(p-tolyl)porphinatoiron(III) t-butoxide

Base Information

Chemical Name:meso-tetra(p-tolyl)porphinatoiron(III) t-butoxide
CAS No.:83970-58-5
Molecular Formula:C₅₂H₄₅FeN₄O
Molecular Weight:797.803
Hs Code.:

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Chemical Property of meso-tetra(p-tolyl)porphinatoiron(III) t-butoxide

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Technology Process of meso-tetra(p-tolyl)porphinatoiron(III) t-butoxide

There total 2 articles about meso-tetra(p-tolyl)porphinatoiron(III) t-butoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87607-84-9
(tetrakis(p-methylphenyl)porphyrin)Fe(C₆H₅)

: 110-05-4
di-tert-butyl peroxide

: 83970-58-5
meso-tetra(p-tolyl)porphinatoiron(III) t-butoxide

Guidance literature:: In ⁽²⁾H₈-toluene; 100°C; 12 h;; identified by 1H NMR spectroscopy;;

Reference yield:

: 19496-18-5
5,10,15,20-tetrakis(4-methylphenyl)porphyrinatoiron(III) chloride

: 865-48-5
sodium t-butanolate

: 83970-58-5
meso-tetra(p-tolyl)porphinatoiron(III) t-butoxide

Guidance literature:: In dichloromethane; tert-butyl alcohol; soln. of the sodium alkoxide added gradually to a CH2Cl2 soln. of TTPFeCl; filtered, evapd. (hot plate), crystals collected (glass frit), washed (hot t-butanol), dried (vac., room temp., 24 h);
DOI:10.1016/S0020-1693(00)80830-0