exo-3-pinanyl-N-phenyl carbamate

Base Information

• Chemical Name: exo-3-pinanyl-N-phenyl carbamate
• CAS No.: 102992-45-0
• Molecular Formula: C₁₇H₂₃NO₂
• Molecular Weight: 273.375
• Mol file: 102992-45-0.mol

Synonyms:

Chemical Property of exo-3-pinanyl-N-phenyl carbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of exo-3-pinanyl-N-phenyl carbamate

There total 6 articles about exo-3-pinanyl-N-phenyl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+)-pinocamphone (18492-59-6) → (1R:2S:3S)-3-phenylcarbamoyloxy-pinane (102992-45-0,133962-57-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium; ethanol / Isolierung ueber den Borsaeureester und das 2-Carboxy-benzoyl-Derivat

With ethanol; sodium;

DOI:10.1021/ja01291a009

Reference yield:

(1R,2R,5S)-2,6,6-trimethylbicyclo[3.1.1]heptan-3-one (473-62-1) → (1R:2S:3S)-3-phenylcarbamoyloxy-pinane (102992-45-0,133962-57-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium; ethanol / Isolierung ueber den Borsaeureester und das 2-Carboxy-benzoyl-Derivat

With ethanol; sodium;

DOI:10.1021/ja01291a009

Reference yield:

(-)-isopinocampheol (1196-00-5) → (1R:2S:3S)-3-phenylcarbamoyloxy-pinane (102992-45-0,133962-57-9)

Guidance literature:

Multi-step reaction with 3 steps

1: CrO₃; aqueous sulfuric acid

2: sodium; ethanol / Isolierung ueber den Borsaeureester und das 2-Carboxy-benzoyl-Derivat

With chromium(VI) oxide; ethanol; sulfuric acid; sodium;

DOI:10.1021/ja01291a009

upstream raw materials:

(1R)-(2endoH)-pinan-3endo-ol

phenyl isocyanate

(-)-isopinocampheol

(+)-pinocamphone

Downstream raw materials:

(4-Hydroxy-phenyl)-carbamic acid (1S,2S,3S,5R,6R)-6-hydroxymethyl-2,6-dimethyl-bicyclo[3.1.1]hept-3-yl ester