Technology Process of C12H17NO5S
There total 4 articles about C12H17NO5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; triethylamine;
In
dichloromethane;
at 0 - 20 ℃;
DOI:10.1021/ml300446a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; triphenylphosphine; tetrabutylammomium bromide / dichloromethane / 12 h / 20 °C
2: tetra-(n-butyl)ammonium iodide; sodium sulfite / ethanol; water / Reflux
3: thionyl chloride / N,N-dimethyl-formamide / 0 - 20 °C
4: triethylamine; dmap / dichloromethane / 0 - 20 °C
With
dmap; thionyl chloride; tetrabutylammomium bromide; tetra-(n-butyl)ammonium iodide; triethylamine; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium sulfite;
In
ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ml300446a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetra-(n-butyl)ammonium iodide; sodium sulfite / ethanol; water / Reflux
2: thionyl chloride / N,N-dimethyl-formamide / 0 - 20 °C
3: triethylamine; dmap / dichloromethane / 0 - 20 °C
With
dmap; thionyl chloride; tetra-(n-butyl)ammonium iodide; triethylamine; sodium sulfite;
In
ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ml300446a