chlorobis(2,6-di-tert-butyl-4-methylphenolato)bis(tetrahydrofuran)ytterbium(III)

Base Information

• Chemical Name: chlorobis(2,6-di-tert-butyl-4-methylphenolato)bis(tetrahydrofuran)ytterbium(III)
• CAS No.: 359860-09-6
• Molecular Formula: C₃₈H₆₂ClO₄Yb
• Molecular Weight: 791.401
• Mol file: 359860-09-6.mol

Synonyms:

Chemical Property of chlorobis(2,6-di-tert-butyl-4-methylphenolato)bis(tetrahydrofuran)ytterbium(III)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of chlorobis(2,6-di-tert-butyl-4-methylphenolato)bis(tetrahydrofuran)ytterbium(III)

There total 1 articles about chlorobis(2,6-di-tert-butyl-4-methylphenolato)bis(tetrahydrofuran)ytterbium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

Yb(2,6-di-tert-butyl-4-methylphenolate)2(THF)3 (166943-03-9,158706-11-7,124206-20-8) + 1,2-dichloro-ethane (107-06-2,52399-93-6) → chlorobis(2,6-di-tert-butyl-4-methylphenolato)bis(tetrahydrofuran)ytterbium(III) (359860-09-6)

Guidance literature:

In tetrahydrofuran; byproducts: C2H4, THF; under Ar or N2, 0.5 equiv. of halogen-compd. was added to Yb-compd. soln. in THF, stirring for 24 h at room temp.; volatiles were removed in vac., solid was dried in vac. at room temp., elem. anal.;

DOI:10.1002/1521-3749(200107)627:7<1652::aid-zaac1652>3.0.co;2-7

upstream raw materials:

Yb(2,6-di-tert-butyl-4-methylphenolate)2(THF)3

1,2-dichloro-ethane

Refernces