C₄₄H₅₄N₂O₆SSi

Base Information

Chemical Name:C₄₄H₅₄N₂O₆SSi
CAS No.:1360744-12-2
Molecular Formula:C₄₄H₅₄N₂O₆SSi
Molecular Weight:767.074
Hs Code.:

C<sub>44</sub>H<sub>54</sub>N<sub>2</sub>O<sub>6</sub>SSi

Synonyms:

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Chemical Property of C₄₄H₅₄N₂O₆SSi

Chemical Property:

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Technology Process of C₄₄H₅₄N₂O₆SSi

There total 11 articles about C₄₄H₅₄N₂O₆SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₃H₅₂N₂O₇SSi

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1360744-12-2
C₄₄H₅₄N₂O₆SSi

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1002/chem.201102101

Reference yield:

: 1360744-09-7
C₁₂H₁₈O₄

: 1360744-12-2
C₄₄H₅₄N₂O₆SSi

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrogen iodide / water; toluene / 0.5 h / 0 - 20 °C

1.2: 2 h / Reflux

2.1: 1H-imidazole; dmap / dichloromethane / 24 h / 20 °C

3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 24 h / -78 - 20 °C

4.1: platinum(II) chloride / toluene / 1.45 h / 80 °C

5.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

5.2: 1 h / 0 - 20 °C

6.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C

6.2: 3 h / 20 °C

7.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / Reflux

8.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 °C

9.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C

With 1H-imidazole; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 2,2'-azobis(isobutyronitrile); dimethylsulfide borane complex; potassium tert-butylate; hydrogen iodide; tri-n-butyl-tin hydride; sodium hydride; diisobutylaluminium hydride; triethylamine; platinum(II) chloride; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene; mineral oil; 3.1: Sonogashira coupling / 5.1: Hydroboration reaction / 7.1: Barton-McCombie deoxygenation / 9.1: Wittig reaction;
DOI:10.1002/chem.201102101

Reference yield:

: 1360744-10-0
C₇H₉IO₂

: 1360744-12-2
C₄₄H₅₄N₂O₆SSi

Guidance literature:: Multi-step reaction with 8 steps

1.1: 1H-imidazole; dmap / dichloromethane / 24 h / 20 °C

2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 24 h / -78 - 20 °C

3.1: platinum(II) chloride / toluene / 1.45 h / 80 °C

4.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

4.2: 1 h / 0 - 20 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C

5.2: 3 h / 20 °C

6.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / Reflux

7.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 °C

8.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C

With 1H-imidazole; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 2,2'-azobis(isobutyronitrile); dimethylsulfide borane complex; potassium tert-butylate; tri-n-butyl-tin hydride; sodium hydride; diisobutylaluminium hydride; triethylamine; platinum(II) chloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil; 2.1: Sonogashira coupling / 4.1: Hydroboration reaction / 6.1: Barton-McCombie deoxygenation / 8.1: Wittig reaction;
DOI:10.1002/chem.201102101