naphthalene-2-methoxycarbonyl-Tyr-Trp-p-hydroxybenzylalcohol

Base Information

Chemical Name:naphthalene-2-methoxycarbonyl-Tyr-Trp-p-hydroxybenzylalcohol
CAS No.:1659291-77-6
Molecular Formula:C₃₉H₃₅N₃O₇
Molecular Weight:657.723
Hs Code.:

Synonyms:

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Chemical Property of naphthalene-2-methoxycarbonyl-Tyr-Trp-p-hydroxybenzylalcohol

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Technology Process of naphthalene-2-methoxycarbonyl-Tyr-Trp-p-hydroxybenzylalcohol

There total 5 articles about naphthalene-2-methoxycarbonyl-Tyr-Trp-p-hydroxybenzylalcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.66%

: 623-05-2
(4-hydroxyphenyl)methanol

: 1616961-29-5
naphthalene-2-methoxycarbonyl-Tyr-Trp-OH

: 1659291-77-6
naphthalene-2-methoxycarbonyl-Tyr-Trp-p-hydroxybenzylalcohol

Guidance literature:: With lipase from Candida rugosa; In water; at 37 ℃; for 720h; pH=7.4; Time; regioselective reaction; Enzymatic reaction;
DOI:10.1039/c4cc02484b

Reference yield:

: 141700-30-3
naphthalene-2-methyloxy chloroformate

: 1659291-77-6
naphthalene-2-methoxycarbonyl-Tyr-Trp-p-hydroxybenzylalcohol

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium carbonate / 1,4-dioxane / 12 h / 20 °C

2.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 12 h / 0 - 20 °C

3.1: sodium hydroxide / methanol / 12 h

3.2: pH 2

4.1: lipase from Candida rugosa / water / 720 h / 37 °C / pH 7.4 / Enzymatic reaction

With lipase from Candida rugosa; sodium carbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium hydroxide; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide;
DOI:10.1039/c4cc02484b

Reference yield:

: 1616961-33-1
Nmoc-Tyr-OH

: 1659291-77-6
naphthalene-2-methoxycarbonyl-Tyr-Trp-p-hydroxybenzylalcohol

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 12 h / 0 - 20 °C

2.1: sodium hydroxide / methanol / 12 h

2.2: pH 2

3.1: lipase from Candida rugosa / water / 720 h / 37 °C / pH 7.4 / Enzymatic reaction

With lipase from Candida rugosa; benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium hydroxide; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1039/c4cc02484b