(Pd(S₂N₂)(P(CH₃)2(C₆H₅))2)

Base Information

Chemical Name:(Pd(S₂N₂)(P(CH₃)2(C₆H₅))2)
CAS No.:110610-52-1
Molecular Formula:C₁₆H₂₂N₂P₂PdS₂
Molecular Weight:474.864
Hs Code.:

(Pd(S<sub>2</sub>N<sub>2</sub>)(P(CH<sub>3</sub>)2(C<sub>6</sub>H<sub>5</sub>))2)

Synonyms:

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Chemical Property of (Pd(S₂N₂)(P(CH₃)2(C₆H₅))2)

Chemical Property:

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Technology Process of (Pd(S₂N₂)(P(CH₃)2(C₆H₅))2)

There total 1 articles about (Pd(S₂N₂)(P(CH₃)2(C₆H₅))2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 293-40-3
tetrasulphur tetraimide

: 29484-74-0,29484-66-0,15616-85-0
dichlorobis(dimethylphenylphosphine)palladium(II)

: 110610-52-1
(Pd(S₂N₂)(P(CH₃)2(C₆H₅))2)

Guidance literature:: With diazabicycloundecane; In dichloromethane; to suspn. of S4N4H4 in a CH2Cl2 soln. of complex was added excess diazabicycloundecane, after 10 min additional diazabicycloundecane was added and react. mixt. stirred for 90 min; CH2Cl2 was removed in vacuo, solid washed with degassed water and dried in vacuo, solid extd. with CH2Cl2 and pptd. using hexane; elem. anal.;
DOI:10.1016/S0277-5387(00)80837-2

Reference yield:

: bromo(di(azathein)-1-yl-S⁽¹⁾N⁽⁴⁾)(dimethylphenylphosphine)platinum(II)

: 110610-52-1
(Pd(S₂N₂)(P(CH₃)2(C₆H₅))2)

: 104185-15-1
cis-Pt(disulphurdinitido)(PMe₂Ph)2

: {Pd(S₂N₂H)(Br)(P(CH₃)2C₆H₅)}

Guidance literature:: In dichloromethane; mixed, allowed to stand overnight; detn. by (31)P-NMR, solvent removed in vac., extn. (warm Et2O), filtration, removal of Et2O, residue taken in CHCl3, slow hexane diffusion; elem. anal.;
DOI:10.1016/S0277-5387(00)80494-5